(E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-3,5-dimethoxy-phenyl)-allyl ester

Base Information

Chemical Name:(E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-3,5-dimethoxy-phenyl)-allyl ester
CAS No.:213185-31-0
Molecular Formula:C₂₄H₂₄O₈
Molecular Weight:440.45
Hs Code.:

Synonyms:(E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-3,5-dimethoxy-phenyl)-allyl ester

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Chemical Property of (E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-3,5-dimethoxy-phenyl)-allyl ester

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Technology Process of (E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-3,5-dimethoxy-phenyl)-allyl ester

There total 3 articles about (E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-3,5-dimethoxy-phenyl)-allyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 53901-95-4,108608-06-6,58523-18-5
p-acetoxycinnamoyl chloride

: 157096-52-1
(E)-3-(4-acetyloxy-3,5-dimethoxyphenyl)-2-propen-1-ol

: 213185-31-0
(E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-3,5-dimethoxy-phenyl)-allyl ester

Guidance literature:: With dmap; triethylamine; In dichloromethane; for 2h;
DOI:10.1021/jf980440y

Reference yield:

: 71686-40-3
(E)-2,6-dimethoxy-4-(3-oxoprop-1-en-1-yl)phenyl acetate

: 213185-31-0
(E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-3,5-dimethoxy-phenyl)-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 94.5 percent / (CH₃)3CNH₂*BH₃ / CH₂Cl₂ / 2 h / Ambient temperature

2: 80 percent / 4-(dimethylamino)pyridine, Et₃N / CH₂Cl₂ / 2 h

With dmap; N-tert-butylaminoborane; triethylamine; In dichloromethane;
DOI:10.1021/jf980440y

Reference yield:

: 27542-85-4
4-acetoxycinnamic acid

: 213185-31-0
(E)-3-(4-Acetoxy-phenyl)-acrylic acid (E)-3-(4-acetoxy-3,5-dimethoxy-phenyl)-allyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: SOCl₂, pyridine

2: 80 percent / 4-(dimethylamino)pyridine, Et₃N / CH₂Cl₂ / 2 h

With pyridine; dmap; thionyl chloride; triethylamine; In dichloromethane;
DOI:10.1021/jf980440y