2-deoxy-2-[[(phenylmethoxy)carbonyl]amino]-D-galactopyranose-1,3,4,6-tetraacetate

Base Information

Chemical Name:2-deoxy-2-[[(phenylmethoxy)carbonyl]amino]-D-galactopyranose-1,3,4,6-tetraacetate
CAS No.:100483-05-4
Molecular Formula:C₂₂H₂₇NO₁₁
Molecular Weight:481.456
Hs Code.:

Synonyms:2-deoxy-2-[[(phenylmethoxy)carbonyl]amino]-D-galactopyranose-1,3,4,6-tetraacetate

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Chemical Property of 2-deoxy-2-[[(phenylmethoxy)carbonyl]amino]-D-galactopyranose-1,3,4,6-tetraacetate

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Technology Process of 2-deoxy-2-[[(phenylmethoxy)carbonyl]amino]-D-galactopyranose-1,3,4,6-tetraacetate

There total 12 articles about 2-deoxy-2-[[(phenylmethoxy)carbonyl]amino]-D-galactopyranose-1,3,4,6-tetraacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 501-53-1,94274-21-2
benzyl chloroformate

: 5432-46-2,1191127-63-5
acetyl 3,4,6-tri-O-acetyl-2-amino-2-deoxy-D-glucopyranoside hydrochloride

: 5348-99-2,35946-66-8,82264-19-5,100483-05-4
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(benzyloxycarbonyl)amino-α/β-D-glucopyranoside

Guidance literature:: With sodium hydrogencarbonate; In dichloromethane; water; at 20 ℃; pH=9;
DOI:10.1002/chem.202005228

Reference yield: 94.0%

: 3006-58-4,13030-01-8,42890-10-8,42973-23-9,77059-32-6,121785-09-9,7474-40-0
2-carbobenzyloxyamino-2-deoxy-D-glucopyranose

: 108-24-7
acetic anhydride

: 5348-99-2,35946-66-8,82264-19-5,100483-05-4
1,3,4,6-tetra-O-acetyl-2-deoxy-2-(benzyloxycarbonyl)amino-α/β-D-glucopyranoside

Guidance literature:: With toluene-4-sulfonic acid; In acetonitrile; at 0 - 40 ℃; for 3h;
DOI:10.1016/j.carres.2008.01.014

Reference yield:

: 90-76-6,90-77-7,530-23-4,579-32-8,579-33-9,643-68-5,2596-19-2,6490-68-2,6490-70-6,6490-72-8,6490-73-9,6490-74-0,14196-84-0,14196-86-2,14257-69-3,58381-21-8
D-galactosamine

: 108-24-7
acetic anhydride

: 501-53-1,94274-21-2
benzyl chloroformate

: 100483-05-4
2-deoxy-2-[[(phenylmethoxy)carbonyl]amino]-D-galactopyranose-1,3,4,6-tetraacetate

Guidance literature:: D-galactosamine; benzyl chloroformate; With sodium hydrogencarbonate; In water; toluene; at 20 ℃; for 3h;

acetic anhydride; With pyridine; at 20 ℃;