3-(5-bromo-1-benzenesulfonyl-1H-indol-3-yl)-1-phenyl-4-(1H-pyrrolo[3,2-b]pyridin-1-yl)-1H-pyrrole-2,5-dione

Base Information

• Chemical Name: 3-(5-bromo-1-benzenesulfonyl-1H-indol-3-yl)-1-phenyl-4-(1H-pyrrolo[3,2-b]pyridin-1-yl)-1H-pyrrole-2,5-dione
• CAS No.: 1178894-39-7
• Molecular Formula: C₃₁H₁₉BrN₄O₄S
• Molecular Weight: 623.486

Synonyms:3-(5-bromo-1-benzenesulfonyl-1H-indol-3-yl)-1-phenyl-4-(1H-pyrrolo[3,2-b]pyridin-1-yl)-1H-pyrrole-2,5-dione

Chemical Property of 3-(5-bromo-1-benzenesulfonyl-1H-indol-3-yl)-1-phenyl-4-(1H-pyrrolo[3,2-b]pyridin-1-yl)-1H-pyrrole-2,5-dione

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Technology Process of 3-(5-bromo-1-benzenesulfonyl-1H-indol-3-yl)-1-phenyl-4-(1H-pyrrolo[3,2-b]pyridin-1-yl)-1H-pyrrole-2,5-dione

There total 1 articles about 3-(5-bromo-1-benzenesulfonyl-1H-indol-3-yl)-1-phenyl-4-(1H-pyrrolo[3,2-b]pyridin-1-yl)-1H-pyrrole-2,5-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.8%

1H-pyrrolo[3,2-b]pyridine (272-49-1) + 3-(5-bromo-1-benzenesulfonyl-1H-indol-3-yl)-4-chloro-1-phenyl-1H-pyrrole-2,5-dione (1178894-34-2) → 3-(5-bromo-1-benzenesulfonyl-1H-indol-3-yl)-1-phenyl-4-(1H-pyrrolo[3,2-b]pyridin-1-yl)-1H-pyrrole-2,5-dione (1178894-39-7)

Guidance literature:

1H-pyrrolo[3,2-b]pyridine; With lithium diisopropyl amide; In tetrahydrofuran; at -10 ℃; for 0.5h; Inert atmosphere;

3-(5-bromo-1-benzenesulfonyl-1H-indol-3-yl)-4-chloro-1-phenyl-1H-pyrrole-2,5-dione; In tetrahydrofuran; at -20 ℃; Inert atmosphere;

DOI:10.1016/j.bmc.2009.05.031

Reference yield: 85.3%

3-(5-bromo-1-benzenesulfonyl-1H-indol-3-yl)-1-phenyl-4-(1H-pyrrolo[3,2-b]pyridin-1-yl)-1H-pyrrole-2,5-dione (1178894-39-7) → 3-(5-bromo-1H-indol-3-yl)-1-phenyl-4-(1H-pyrrolo[3,2-b]pyridin-1-yl)-1H-pyrrole-2,5-dione (1178894-44-4)

Guidance literature:

With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 2h;

DOI:10.1016/j.bmc.2009.05.031

upstream raw materials:

1H-pyrrolo[3,2-b]pyridine

3-(5-bromo-1-benzenesulfonyl-1H-indol-3-yl)-4-chloro-1-phenyl-1H-pyrrole-2,5-dione

Downstream raw materials:

3-(5-bromo-1H-indol-3-yl)-1-phenyl-4-(1H-pyrrolo[3,2-b]pyridin-1-yl)-1H-pyrrole-2,5-dione

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