1-[(2R,3S)-2-(2,4-Dichloro-phenyl)-3-methyl-oxiranylmethyl]-1H-[1,2,4]triazole

Base Information

Chemical Name:1-[(2R,3S)-2-(2,4-Dichloro-phenyl)-3-methyl-oxiranylmethyl]-1H-[1,2,4]triazole
CAS No.:132563-76-9
Molecular Formula:C₁₂H₁₁Cl₂N₃O
Molecular Weight:284.145
Hs Code.:

Synonyms:1-[(2R,3S)-2-(2,4-Dichloro-phenyl)-3-methyl-oxiranylmethyl]-1H-[1,2,4]triazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-[(2R,3S)-2-(2,4-Dichloro-phenyl)-3-methyl-oxiranylmethyl]-1H-[1,2,4]triazole

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Technology Process of 1-[(2R,3S)-2-(2,4-Dichloro-phenyl)-3-methyl-oxiranylmethyl]-1H-[1,2,4]triazole

There total 4 articles about 1-[(2R,3S)-2-(2,4-Dichloro-phenyl)-3-methyl-oxiranylmethyl]-1H-[1,2,4]triazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 127181-89-9
Methanesulfonic acid (1R,2R)-2-(2,4-dichloro-phenyl)-2-hydroxy-1-methyl-3-[1,2,4]triazol-1-yl-propyl ester

: 132563-76-9
1-[(2R,3S)-2-(2,4-Dichloro-phenyl)-3-methyl-oxiranylmethyl]-1H-[1,2,4]triazole

Guidance literature:: With sodium azide; ammonium chloride; In N,N-dimethyl-formamide; at 115 ℃; for 0.5h;
DOI:10.1248/cpb.38.2476

Reference yield:

: 126916-48-1,127181-89-9,132563-74-7
Methanesulfonic acid (1S,2S)-2-(2,4-dichloro-phenyl)-2-hydroxy-1-methyl-3-[1,2,4]triazol-1-yl-propyl ester

: 126916-92-5,132507-90-5,132563-76-9,132563-79-2
1-[(2S,3R)-2-(2,4-Dichloro-phenyl)-3-methyl-oxiranylmethyl]-1H-[1,2,4]triazole

Guidance literature:: With sodium azide; ammonium chloride; In N,N-dimethyl-formamide; at 115 ℃; for 0.5h;
DOI:10.1248/cpb.38.2476

Reference yield:

: 127181-87-7
(2R,3R)-2-(2,4-Dichlorophenyl)-1-(1H-1,2,4-triazol-1-yl)-2,3-butanediol

: 132563-76-9
1-[(2R,3S)-2-(2,4-Dichloro-phenyl)-3-methyl-oxiranylmethyl]-1H-[1,2,4]triazole

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / pyridine / 2 h / Ambient temperature

2: 80 percent / NaN₃, NH₄Cl / dimethylformamide / 0.5 h / 115 °C

With pyridine; sodium azide; ammonium chloride; In N,N-dimethyl-formamide;
DOI:10.1248/cpb.38.2476