3-phenyl-7-hydroxy-5-heptenal

Base Information

Chemical Name:3-phenyl-7-hydroxy-5-heptenal
CAS No.:692728-74-8
Molecular Formula:C₁₃H₁₆O₂
Molecular Weight:204.269
Hs Code.:

Synonyms:3-phenyl-7-hydroxy-5-heptenal

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-phenyl-7-hydroxy-5-heptenal

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Technology Process of 3-phenyl-7-hydroxy-5-heptenal

There total 10 articles about 3-phenyl-7-hydroxy-5-heptenal which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 692728-73-7
(E)-3-Phenyl-7-(tetrahydro-pyran-2-yloxy)-hept-5-enal

: 692728-74-8
3-phenyl-7-hydroxy-5-heptenal

Guidance literature:: With hydrogenchloride; In tetrahydrofuran;
DOI:10.1016/j.tetlet.2004.02.058

Reference yield:

: 4407-36-7
(2E)-3-phenyl-2-propen-1-ol

: 692728-74-8
3-phenyl-7-hydroxy-5-heptenal

Guidance literature:: Multi-step reaction with 11 steps

1.1: 70 percent / p-TsOH / xylene

2.1: LiAlH₄ / tetrahydrofuran

3.1: imidazole / dimethylformamide

4.1: BH₃/SMe₂ / tetrahydrofuran

4.2: 63 percent / H₂O₂; NaOH / tetrahydrofuran

5.1: (COCl)2; Et₃N / dimethylsulfoxide; CH₂Cl₂

6.1: NaH / tetrahydrofuran

7.1: DIBAL-H / tetrahydrofuran

8.1: p-TsOH / CH₂Cl₂

9.1: TBAF / tetrahydrofuran

10.1: 80 percent / Dess-Martin periodinane / CH₂Cl₂

11.1: 91 percent / HCl / tetrahydrofuran

With 1H-imidazole; hydrogenchloride; lithium aluminium tetrahydride; oxalyl dichloride; dimethylsulfide; borane; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; xylene; 1.1: Johnson-Claisen rearrangement / 5.1: Swern oxidation / 6.1: Emmons-Horner reaction;
DOI:10.1016/j.tetlet.2004.02.058

Reference yield:

: 80816-30-4
3-phenyl-4-pentenol

: 692728-74-8
3-phenyl-7-hydroxy-5-heptenal

Guidance literature:: Multi-step reaction with 9 steps

1.1: imidazole / dimethylformamide

2.1: BH₃/SMe₂ / tetrahydrofuran

2.2: 63 percent / H₂O₂; NaOH / tetrahydrofuran

3.1: (COCl)2; Et₃N / dimethylsulfoxide; CH₂Cl₂

4.1: NaH / tetrahydrofuran

5.1: DIBAL-H / tetrahydrofuran

6.1: p-TsOH / CH₂Cl₂

7.1: TBAF / tetrahydrofuran

8.1: 80 percent / Dess-Martin periodinane / CH₂Cl₂

9.1: 91 percent / HCl / tetrahydrofuran

With 1H-imidazole; hydrogenchloride; oxalyl dichloride; dimethylsulfide; borane; tetrabutyl ammonium fluoride; sodium hydride; diisobutylaluminium hydride; Dess-Martin periodane; toluene-4-sulfonic acid; triethylamine; In tetrahydrofuran; dichloromethane; dimethyl sulfoxide; N,N-dimethyl-formamide; 3.1: Swern oxidation / 4.1: Emmons-Horner reaction;
DOI:10.1016/j.tetlet.2004.02.058