2,3-Bis-chloromethyl-6,9-dimethoxy-7,8-dinitro-2a,10b-diphenyl-2a,5,10,10b-tetrahydro-2H,3H-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulene-1,4-dione

Base Information

Chemical Name:2,3-Bis-chloromethyl-6,9-dimethoxy-7,8-dinitro-2a,10b-diphenyl-2a,5,10,10b-tetrahydro-2H,3H-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulene-1,4-dione
CAS No.:188427-73-8
Molecular Formula:C₂₈H₂₄Cl₂N₆O₈
Molecular Weight:643.44
Hs Code.:

2,3-Bis-chloromethyl-6,9-dimethoxy-7,8-dinitro-2a,10b-diphenyl-2a,5,10,10b-tetrahydro-2H,3H-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulene-1,4-dione

Synonyms:2,3-Bis-chloromethyl-6,9-dimethoxy-7,8-dinitro-2a,10b-diphenyl-2a,5,10,10b-tetrahydro-2H,3H-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulene-1,4-dione

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,3-Bis-chloromethyl-6,9-dimethoxy-7,8-dinitro-2a,10b-diphenyl-2a,5,10,10b-tetrahydro-2H,3H-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulene-1,4-dione

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

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Technology Process of 2,3-Bis-chloromethyl-6,9-dimethoxy-7,8-dinitro-2a,10b-diphenyl-2a,5,10,10b-tetrahydro-2H,3H-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulene-1,4-dione

There total 8 articles about 2,3-Bis-chloromethyl-6,9-dimethoxy-7,8-dinitro-2a,10b-diphenyl-2a,5,10,10b-tetrahydro-2H,3H-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulene-1,4-dione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 188427-72-7
Acetic acid 3-acetoxymethyl-6,9-dimethoxy-7,8-dinitro-1,4-dioxo-2a,10b-diphenyl-2a,3,4,5,10,10b-hexahydro-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulen-2-ylmethyl ester

: 188427-73-8
2,3-Bis-chloromethyl-6,9-dimethoxy-7,8-dinitro-2a,10b-diphenyl-2a,5,10,10b-tetrahydro-2H,3H-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulene-1,4-dione

Guidance literature:: With thionyl chloride; In dichloromethane; for 16h;
DOI:10.1021/jo961382n

Reference yield:

: 146443-42-7
1,3,4,6-Tetrakis(chloromethyl)tetrahydro-3a,6a-diphenylimidazo<4,5-d>imidazole-2,5(1H,3H)-dione

: 188427-73-8
2,3-Bis-chloromethyl-6,9-dimethoxy-7,8-dinitro-2a,10b-diphenyl-2a,5,10,10b-tetrahydro-2H,3H-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulene-1,4-dione

Guidance literature:: Multi-step reaction with 7 steps

1: SnCl₄ / 1,2-dichloro-ethane / -35 - 0 °C

2: 65 percent / p-TsOH*H₂O / Heating

3: 88 percent / SnCl₄ / 1,2-dichloro-ethane / -35 - 0 °C

4: 80 percent / 53percent HNO₃ / acetic anhydride / 16 h / Ambient temperature

5: 94 percent / 53percent HNO₃ / acetic anhydride / 16 h / Ambient temperature

6: 95 percent / p-TsOH*H₂O / 3 h / 110 °C

7: 100 percent / SOCl₂ / CH₂Cl₂ / 16 h

With thionyl chloride; nitric acid; tin(IV) chloride; toluene-4-sulfonic acid; In dichloromethane; acetic anhydride; 1,2-dichloro-ethane;
DOI:10.1021/jo961382n

Reference yield:

: 150-78-7
1,4-dimethoxybezene

: 188427-73-8
2,3-Bis-chloromethyl-6,9-dimethoxy-7,8-dinitro-2a,10b-diphenyl-2a,5,10,10b-tetrahydro-2H,3H-2,3,4a,10a-tetraaza-benzo[g]cyclopenta[cd]azulene-1,4-dione

Guidance literature:: Multi-step reaction with 5 steps

1: 58 percent / SnCl₄ / 1,2-dichloro-ethane / -35 - 0 °C

2: 80 percent / 53percent HNO₃ / acetic anhydride / 16 h / Ambient temperature

3: 94 percent / 53percent HNO₃ / acetic anhydride / 16 h / Ambient temperature

4: 95 percent / p-TsOH*H₂O / 3 h / 110 °C

5: 100 percent / SOCl₂ / CH₂Cl₂ / 16 h

With thionyl chloride; nitric acid; tin(IV) chloride; toluene-4-sulfonic acid; In dichloromethane; acetic anhydride; 1,2-dichloro-ethane;
DOI:10.1021/jo961382n