1,1,3,3-tetramethyl-1,3-bis(N-methyl-N'-tosyl-(S)-prolinamidomethyl)-1,3-disiloxane

Base Information

Chemical Name:1,1,3,3-tetramethyl-1,3-bis(N-methyl-N'-tosyl-(S)-prolinamidomethyl)-1,3-disiloxane
CAS No.:1375314-04-7
Molecular Formula:C₃₂H₅₀N₄O₇S₂Si₂
Molecular Weight:723.075
Hs Code.:

Synonyms:1,1,3,3-tetramethyl-1,3-bis(N-methyl-N'-tosyl-(S)-prolinamidomethyl)-1,3-disiloxane

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Chemical Property of 1,1,3,3-tetramethyl-1,3-bis(N-methyl-N'-tosyl-(S)-prolinamidomethyl)-1,3-disiloxane

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Technology Process of 1,1,3,3-tetramethyl-1,3-bis(N-methyl-N'-tosyl-(S)-prolinamidomethyl)-1,3-disiloxane

There total 4 articles about 1,1,3,3-tetramethyl-1,3-bis(N-methyl-N'-tosyl-(S)-prolinamidomethyl)-1,3-disiloxane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: N-(dimethylchlorosilylmethyl)-N-methyl-N'-tosyl-(S)-prolinamide

: 1375314-04-7
1,1,3,3-tetramethyl-1,3-bis(N-methyl-N'-tosyl-(S)-prolinamidomethyl)-1,3-disiloxane

Guidance literature:: With water; sodium hydrogencarbonate; In chloroform; for 24h;
DOI:10.1007/s10593-012-0949-7

Reference yield:

: 52060-82-9
L-proline methylamide

: 1375314-04-7
1,1,3,3-tetramethyl-1,3-bis(N-methyl-N'-tosyl-(S)-prolinamidomethyl)-1,3-disiloxane

Guidance literature:: Multi-step reaction with 3 steps

1: triethylamine / diethyl ether / 4 h / Reflux

2: benzene / 8 h

3: water; sodium hydrogencarbonate / chloroform / 24 h

With water; sodium hydrogencarbonate; triethylamine; In diethyl ether; chloroform; benzene;
DOI:10.1007/s10593-012-0949-7

Reference yield:

: 920323-94-0
N-(p-tosyl)proline N'-methylamide

: 1375314-04-7
1,1,3,3-tetramethyl-1,3-bis(N-methyl-N'-tosyl-(S)-prolinamidomethyl)-1,3-disiloxane

Guidance literature:: Multi-step reaction with 2 steps

1: 1,1,1,3,3,3-hexamethyl-disilazane / toluene / 8 h / Reflux

2: water; sodium hydrogencarbonate / chloroform / 24 h

With water; sodium hydrogencarbonate; 1,1,1,3,3,3-hexamethyl-disilazane; In chloroform; toluene;
DOI:10.1007/s10593-012-0949-7