C₄₈H₆₈O₉Si

Base Information

Chemical Name:C₄₈H₆₈O₉Si
CAS No.:1380328-02-8
Molecular Formula:C₄₈H₆₈O₉Si
Molecular Weight:817.148
Hs Code.:

C<sub>48</sub>H<sub>68</sub>O<sub>9</sub>Si

Synonyms:C₄₈H₆₈O₉Si

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Chemical Property of C₄₈H₆₈O₉Si

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Technology Process of C₄₈H₆₈O₉Si

There total 13 articles about C₄₈H₆₈O₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: C₄₉H₇₀O₇Si

: 1380328-02-8
C₄₈H₆₈O₉Si

Guidance literature:: With potassium permanganate; sodium periodate; In tert-butyl alcohol; at 20 ℃; for 17h; pH=7.2; aq. phosphate buffer; Inert atmosphere;
DOI:10.1021/jm300566h

Reference yield:

: 1380327-94-5
C₃₈H₅₆O₄S₂

: 1380328-02-8
C₄₈H₆₈O₉Si

Guidance literature:: Multi-step reaction with 6 steps

1.1: water; toluene-4-sulfonic acid / tetrahydrofuran; water; acetonitrile / 2 h / 20 °C

2.1: mercury(II) perchlorate hexahydrate / dichloromethane; water; acetonitrile / 1 h / 4 °C

3.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 2 h / 20 °C

3.2: 1 h / 50 °C

4.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C

5.1: 1H-imidazole / tetrahydrofuran / 1 h / 20 °C

6.1: sodium periodate; potassium permanganate / tert-butyl alcohol / 17 h / 20 °C / pH 7.2 / aq. phosphate buffer; Inert atmosphere

With 1H-imidazole; potassium permanganate; sodium periodate; mercury(II) perchlorate hexahydrate; 2,4,6-trichlorobenzoyl chloride; water; toluene-4-sulfonic acid; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1021/jm300566h

Reference yield:

: C₃₅H₅₂O₄S₂

: 1380328-02-8
C₄₈H₆₈O₉Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: tetrapropylammonium perruthennate; 4-methylmorpholine N-oxide / dichloromethane / 0.25 h / 20 °C / Molecular sieve

2.1: tetrahydrofuran; diethyl ether / 0.5 h / -78 °C / Inert atmosphere

3.1: water; toluene-4-sulfonic acid / tetrahydrofuran; water; acetonitrile / 2 h / 20 °C

4.1: mercury(II) perchlorate hexahydrate / dichloromethane; water; acetonitrile / 1 h / 4 °C

5.1: 2,4,6-trichlorobenzoyl chloride; triethylamine / toluene / 2 h / 20 °C

5.2: 1 h / 50 °C

6.1: water; 2,3-dicyano-5,6-dichloro-p-benzoquinone / dichloromethane / 1 h / 20 °C

7.1: 1H-imidazole / tetrahydrofuran / 1 h / 20 °C

8.1: sodium periodate; potassium permanganate / tert-butyl alcohol / 17 h / 20 °C / pH 7.2 / aq. phosphate buffer; Inert atmosphere

With 1H-imidazole; potassium permanganate; sodium periodate; tetrapropylammonium perruthennate; mercury(II) perchlorate hexahydrate; 2,4,6-trichlorobenzoyl chloride; water; toluene-4-sulfonic acid; 4-methylmorpholine N-oxide; triethylamine; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In tetrahydrofuran; diethyl ether; dichloromethane; water; toluene; acetonitrile; tert-butyl alcohol;
DOI:10.1021/jm300566h