N-(2-(2-methyl-2-(benzylthio)propylcarbamoyl)propan-2-yl)-3-methyl-3-(benzylthio)butanamide

Base Information

Chemical Name:N-(2-(2-methyl-2-(benzylthio)propylcarbamoyl)propan-2-yl)-3-methyl-3-(benzylthio)butanamide
CAS No.:1313762-27-4
Molecular Formula:C₂₇H₃₈N₂O₂S₂
Molecular Weight:486.743
Hs Code.:

Synonyms:N-(2-(2-methyl-2-(benzylthio)propylcarbamoyl)propan-2-yl)-3-methyl-3-(benzylthio)butanamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(2-(2-methyl-2-(benzylthio)propylcarbamoyl)propan-2-yl)-3-methyl-3-(benzylthio)butanamide

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Technology Process of N-(2-(2-methyl-2-(benzylthio)propylcarbamoyl)propan-2-yl)-3-methyl-3-(benzylthio)butanamide

There total 6 articles about N-(2-(2-methyl-2-(benzylthio)propylcarbamoyl)propan-2-yl)-3-methyl-3-(benzylthio)butanamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

: 1313762-26-3
2-(3-(benzylthio)-3-methylbutanamido)-2-methylpropanoic acid

: 59681-09-3
2-benzylthio 2-methyl propylamine

: 1313762-27-4
N-(2-(2-methyl-2-(benzylthio)propylcarbamoyl)propan-2-yl)-3-methyl-3-(benzylthio)butanamide

Guidance literature:: With O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 20 ℃; for 18h; Inert atmosphere;
DOI:10.1007/s00775-011-0794-7

Reference yield:

: 100-53-8
phenylmethanethiol

: 1313762-27-4
N-(2-(2-methyl-2-(benzylthio)propylcarbamoyl)propan-2-yl)-3-methyl-3-(benzylthio)butanamide

Guidance literature:: Multi-step reaction with 3 steps

1: piperidine / benzene / 10 h / Reflux; Inert atmosphere

2: lithium aluminium tetrahydride / tetrahydrofuran / 15 h / 20 °C / Cooling with acetone-dry ice; Inert atmosphere

3: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

With piperidine; lithium aluminium tetrahydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; benzene;
DOI:10.1007/s00775-011-0794-7

Reference yield:

: 105780-12-9
benzyl(2-methyl-1-nitropropan-2-yl)sulfane

: 1313762-27-4
N-(2-(2-methyl-2-(benzylthio)propylcarbamoyl)propan-2-yl)-3-methyl-3-(benzylthio)butanamide

Guidance literature:: Multi-step reaction with 2 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / 15 h / 20 °C / Cooling with acetone-dry ice; Inert atmosphere

2: O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 18 h / 20 °C / Inert atmosphere

With lithium aluminium tetrahydride; O-(1H-benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1007/s00775-011-0794-7