2-(Benzhydrylidene-amino)-3-(4-ethoxycarbonylmethyl-phenyl)-propionic acid ethyl ester

Base Information

Chemical Name:2-(Benzhydrylidene-amino)-3-(4-ethoxycarbonylmethyl-phenyl)-propionic acid ethyl ester
CAS No.:156143-76-9
Molecular Formula:C₂₈H₂₉NO₄
Molecular Weight:443.543
Hs Code.:

Synonyms:2-(Benzhydrylidene-amino)-3-(4-ethoxycarbonylmethyl-phenyl)-propionic acid ethyl ester

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Chemical Property of 2-(Benzhydrylidene-amino)-3-(4-ethoxycarbonylmethyl-phenyl)-propionic acid ethyl ester

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Technology Process of 2-(Benzhydrylidene-amino)-3-(4-ethoxycarbonylmethyl-phenyl)-propionic acid ethyl ester

There total 1 articles about 2-(Benzhydrylidene-amino)-3-(4-ethoxycarbonylmethyl-phenyl)-propionic acid ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 69555-14-2
ethyl N-diphenylmethylene glycine

: 7398-81-4
(4-bromomethylphenyl)acetic acid ethyl ester

: 156143-76-9
2-(Benzhydrylidene-amino)-3-(4-ethoxycarbonylmethyl-phenyl)-propionic acid ethyl ester

Guidance literature:: With N-benzyl-trimethylammonium hydroxide; potassium iodide; In 1,4-dioxane; water; for 3h; Ambient temperature;
DOI:10.1021/jm00035a014

Reference yield: 83.0%

: 156143-76-9
2-(Benzhydrylidene-amino)-3-(4-ethoxycarbonylmethyl-phenyl)-propionic acid ethyl ester

: 156143-77-0
2-Amino-3-(4-ethoxycarbonylmethyl-phenyl)-propionic acid ethyl ester

Guidance literature:: With hydrogenchloride; In diethyl ether; for 4h; Ambient temperature;
DOI:10.1021/jm00035a014

Reference yield:

: 156143-76-9
2-(Benzhydrylidene-amino)-3-(4-ethoxycarbonylmethyl-phenyl)-propionic acid ethyl ester

: 156143-99-6
(R,S)-1,1'-dithiobis<2-amino-3-<4-(carboxymethyl)cyclohexyl>propane>, bis(trifluoroacetate)

Guidance literature:: Multi-step reaction with 7 steps

1: 83 percent / 1 N aq. HCl / diethyl ether / 4 h / Ambient temperature

2: 100 percent / H₂, 80percent aq. AcOH / PtO₂ / 80 °C / 60004.8 Torr

3: 96 percent / dimethylformamide

4: 39 percent / NaBH₄ / ethanol; H₂O / 4 h / 50 °C

5: 67 percent / PPh₃, diisopropyl azodicarboxylate / tetrahydrofuran / Ambient temperature

6: 1.) 1 N NaOH, 2.) I₂ / 1.) EtOH, a) 0 deg C, 30 min, b) RT, 3 h, 2.) EtOH

7: 69 percent / anisole / CH₂Cl₂ / 1.) 0 deg C, 30 min, 2.) RT, 2 h

With hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; di-isopropyl azodicarboxylate; hydrogen; iodine; acetic acid; methoxybenzene; triphenylphosphine; platinum(IV) oxide; In tetrahydrofuran; diethyl ether; ethanol; dichloromethane; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00035a014