C₂₁H₃₄O

Base Information Edit

Chemical Name:C₂₁H₃₄O
CAS No.:1428957-10-1
Molecular Formula:C₂₁H₃₄O
Molecular Weight:302.5
Hs Code.:
Mol file:1428957-10-1.mol

Synonyms:C₂₁H₃₄O

Suppliers and Price of C₂₁H₃₄O

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Chemical Property of C₂₁H₃₄O Edit

Chemical Property:

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Technology Process of C₂₁H₃₄O

There total 14 articles about C₂₁H₃₄O which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-94-1,11119-77-0,9003-41-2,9075-99-4
cyclohexanone

: 1428957-10-1
C₂₁H₃₄O

Guidance literature:: Multi-step reaction with 15 steps

1.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C

1.2: -40 - 20 °C

2.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

3.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

4.1: sodium ethanolate / ethanol / 0 °C

4.2: 16 h / 0 - 20 °C

5.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C

6.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C

6.2: -40 - 20 °C

7.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

8.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

9.1: sodium ethanolate / ethanol / 0 °C / Inert atmosphere

9.2: 16 h / 0 - 20 °C

10.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C

11.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0.25 h / 0 °C

11.2: -40 - 20 °C

12.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

13.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

14.1: sodium ethanolate / ethanol / 0 °C

14.2: 16 h / 0 - 20 °C

15.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C

With lithium aluminium tetrahydride; 15-crown-5; sodium ethanolate; phosphorus tribromide; sodium hydride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; mineral oil;

Reference yield:

: 1552-92-7
ethyl cyclohexylideneacetate

: 1428957-10-1
C₂₁H₃₄O

Guidance literature:: Multi-step reaction with 14 steps

1.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

2.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

3.1: sodium ethanolate / ethanol / 0 °C

3.2: 16 h / 0 - 20 °C

4.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C

5.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C

5.2: -40 - 20 °C

6.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

7.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

8.1: sodium ethanolate / ethanol / 0 °C / Inert atmosphere

8.2: 16 h / 0 - 20 °C

9.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C

10.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0.25 h / 0 °C

10.2: -40 - 20 °C

11.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

12.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

13.1: sodium ethanolate / ethanol / 0 °C

13.2: 16 h / 0 - 20 °C

14.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C

With lithium aluminium tetrahydride; 15-crown-5; sodium ethanolate; phosphorus tribromide; sodium hydride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; mineral oil;

Reference yield:

: 932-89-8
2-cyclohexylidene ethanol

: 1428957-10-1
C₂₁H₃₄O

Guidance literature:: Multi-step reaction with 13 steps

1.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

2.1: sodium ethanolate / ethanol / 0 °C

2.2: 16 h / 0 - 20 °C

3.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C

4.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0 °C

4.2: -40 - 20 °C

5.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

6.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

7.1: sodium ethanolate / ethanol / 0 °C / Inert atmosphere

7.2: 16 h / 0 - 20 °C

8.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C

9.1: sodium hydride; 15-crown-5 / tetrahydrofuran; mineral oil / 0.25 h / 0 °C

9.2: -40 - 20 °C

10.1: lithium aluminium tetrahydride / tetrahydrofuran / 0 °C / Inert atmosphere

11.1: phosphorus tribromide / diethyl ether / 0 °C / Inert atmosphere

12.1: sodium ethanolate / ethanol / 0 °C

12.2: 16 h / 0 - 20 °C

13.1: potassium hydroxide / methanol; water / 2 h / 80 - 85 °C

With lithium aluminium tetrahydride; 15-crown-5; sodium ethanolate; phosphorus tribromide; sodium hydride; potassium hydroxide; In tetrahydrofuran; methanol; diethyl ether; ethanol; water; mineral oil;