Technology Process of C27H34N2O8
There total 3 articles about C27H34N2O8 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
(2S)-2-[(tert-butoxycarbonyl)amino]-2-phenylethanoic acid;
With
4-methyl-morpholine; isobutyl chloroformate;
In
tetrahydrofuran;
at -15 ℃;
for 0.75h;
Schlenk technique;
Inert atmosphere;
methyl 2-amino-2-deoxy-4,6-O-(phenylmethylene)-α-D-mannopyranoside;
In
tetrahydrofuran; toluene;
at 20 ℃;
for 2h;
Schlenk technique;
Inert atmosphere;
DOI:10.1002/adsc.201301112
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium azide / N,N-dimethyl-formamide / 70 °C
2.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 35 °C
3.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.75 h / -15 °C / Schlenk technique; Inert atmosphere
3.2: 2 h / 20 °C / Schlenk technique; Inert atmosphere
With
4-methyl-morpholine; lithium aluminium tetrahydride; sodium azide; isobutyl chloroformate;
In
tetrahydrofuran; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1002/adsc.201301112
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: lithium aluminium tetrahydride / diethyl ether / 2 h / 35 °C
2.1: 4-methyl-morpholine; isobutyl chloroformate / tetrahydrofuran / 0.75 h / -15 °C / Schlenk technique; Inert atmosphere
2.2: 2 h / 20 °C / Schlenk technique; Inert atmosphere
With
4-methyl-morpholine; lithium aluminium tetrahydride; isobutyl chloroformate;
In
tetrahydrofuran; diethyl ether;
DOI:10.1002/adsc.201301112