(-)-2'',6''-dimethoxy-2,2'-diphenyl-2,2'-dicyclohexanol

Base Information

Chemical Name:(-)-2'',6''-dimethoxy-2,2'-diphenyl-2,2'-dicyclohexanol
CAS No.:169768-32-5
Molecular Formula:C₃₄H₄₂O₆
Molecular Weight:546.704
Hs Code.:

(-)-2'',6''-dimethoxy-2,2'-diphenyl-2,2'-<m-phenylenebis(methyleneoxy)>dicyclohexanol

Synonyms:(-)-2'',6''-dimethoxy-2,2'-diphenyl-2,2'-dicyclohexanol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (-)-2'',6''-dimethoxy-2,2'-diphenyl-2,2'-dicyclohexanol

Chemical Property:

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Technology Process of (-)-2'',6''-dimethoxy-2,2'-diphenyl-2,2'-dicyclohexanol

There total 3 articles about (-)-2'',6''-dimethoxy-2,2'-diphenyl-2,2'-dicyclohexanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 169872-70-2
(-)-2,5-dimethoxy-1,3-bis(2'-methoxymethoxy-1'-phenylcyclohexyloxymethyl)benzene

: 169768-32-5
(-)-2'',6''-dimethoxy-2,2'-diphenyl-2,2'-dicyclohexanol

Guidance literature:: With hydrogenchloride; In methanol; at 50 ℃; for 3h;
DOI:10.1039/P19950001429

Reference yield:

: 34281-90-8
(1S,2S)-1-phenyl-1,2-cyclohexanediol

: 169768-32-5
(-)-2'',6''-dimethoxy-2,2'-diphenyl-2,2'-dicyclohexanol

Guidance literature:: Multi-step reaction with 3 steps

1: 3.50 g / LiBr, TsOH / 9 h / Heating

2: 94 percent / NaH / tetrahydrofuran / 1.) room temperature, 1 h, 2.) reflux, 24 h

3: 86 percent / conc. HCl / methanol / 3 h / 50 °C

With hydrogenchloride; sodium hydride; toluene-4-sulfonic acid; lithium bromide; In tetrahydrofuran; methanol;
DOI:10.1039/P19950001429

Reference yield:

: 169872-69-9
(+)-2-methoxymethoxy-1-phenylcyclohexanol

: 169768-32-5
(-)-2'',6''-dimethoxy-2,2'-diphenyl-2,2'-dicyclohexanol

Guidance literature:: Multi-step reaction with 2 steps

1: 94 percent / NaH / tetrahydrofuran / 1.) room temperature, 1 h, 2.) reflux, 24 h

2: 86 percent / conc. HCl / methanol / 3 h / 50 °C

With hydrogenchloride; sodium hydride; In tetrahydrofuran; methanol;
DOI:10.1039/P19950001429