Technology Process of C26H39N3O3
There total 15 articles about C26H39N3O3 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 9 steps
1: Jones reagent / acetone
2: diethyl ether
3: potassium hydroxide / ethanol
4: potassium hydroxide
5: 20 % Pd(OH)2/C; hydrogen
7: methanol / 55 °C
8: hydrogenchloride / water / 55 °C
9: acetic acid / toluene / 80 °C
With
hydrogenchloride; Jones reagent; 20 % Pd(OH)2/C; hydrogen; acetic acid; potassium hydroxide;
In
methanol; diethyl ether; ethanol; water; acetone; toluene;
7: Ugi condensation;
DOI:10.1016/j.bmcl.2010.12.109
- Guidance literature:
-
Multi-step reaction with 13 steps
1: sulfuric acid / methanol
2: diisobutylaluminium hydride / tetrahydrofuran
3: titanium(IV) isopropylate; diethyl (2R,3R)-tartrate; Cumene hydroperoxide / dichloromethane / Molecular sieve
4: sodium hydride / tetrahydrofuran
5: Jones reagent / acetone
6: diethyl ether
7: potassium hydroxide / ethanol
8: potassium hydroxide
9: 20 % Pd(OH)2/C; hydrogen
11: methanol / 55 °C
12: hydrogenchloride / water / 55 °C
13: acetic acid / toluene / 80 °C
With
titanium(IV) isopropylate; hydrogenchloride; Jones reagent; diethyl (2R,3R)-tartrate; Cumene hydroperoxide; sulfuric acid; 20 % Pd(OH)2/C; hydrogen; sodium hydride; diisobutylaluminium hydride; acetic acid; potassium hydroxide;
In
tetrahydrofuran; methanol; diethyl ether; ethanol; dichloromethane; water; acetone; toluene;
3: Sharpless epoxidation / 11: Ugi condensation;
DOI:10.1016/j.bmcl.2010.12.109
