(E)-2-(2,6-dinitro-4-(trifluoromethyl)phenoxy)benzaldehyde O-(2,4-dichlorobenzyl) oxime

Base Information

Chemical Name:(E)-2-(2,6-dinitro-4-(trifluoromethyl)phenoxy)benzaldehyde O-(2,4-dichlorobenzyl) oxime
CAS No.:1377291-15-0
Molecular Formula:C₂₁H₁₂Cl₂F₃N₃O₆
Molecular Weight:530.244
Hs Code.:

Synonyms:(E)-2-(2,6-dinitro-4-(trifluoromethyl)phenoxy)benzaldehyde O-(2,4-dichlorobenzyl) oxime

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Chemical Property of (E)-2-(2,6-dinitro-4-(trifluoromethyl)phenoxy)benzaldehyde O-(2,4-dichlorobenzyl) oxime

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Technology Process of (E)-2-(2,6-dinitro-4-(trifluoromethyl)phenoxy)benzaldehyde O-(2,4-dichlorobenzyl) oxime

There total 4 articles about (E)-2-(2,6-dinitro-4-(trifluoromethyl)phenoxy)benzaldehyde O-(2,4-dichlorobenzyl) oxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 393-75-9
4-chloro-3,5-dinitrobenzotrifluoride

: C₁₄H₁₁Cl₂NO₂

: 1377291-15-0
(E)-2-(2,6-dinitro-4-(trifluoromethyl)phenoxy)benzaldehyde O-(2,4-dichlorobenzyl) oxime

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 - 60 ℃; for 1h;
DOI:10.1016/j.bmc.2012.03.057

Reference yield:

: 98-56-6
4-chlorobenzotrifluoride

: 1377291-15-0
(E)-2-(2,6-dinitro-4-(trifluoromethyl)phenoxy)benzaldehyde O-(2,4-dichlorobenzyl) oxime

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid; sulfur trioxide; nitric acid / 3 h / 50 - 70 °C

2: sulfuric acid; sulfur trioxide; nitric acid / 2 h / 100 - 115 °C

3: potassium carbonate / N,N-dimethyl-formamide / 1 h / 50 - 60 °C

With sulfuric acid; sulfur trioxide; nitric acid; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.03.057

Reference yield:

: 121-17-5
2-chloro-3-nitro-5-trifluoromethylbenzene

: 1377291-15-0
(E)-2-(2,6-dinitro-4-(trifluoromethyl)phenoxy)benzaldehyde O-(2,4-dichlorobenzyl) oxime

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuric acid; sulfur trioxide; nitric acid / 2 h / 100 - 115 °C

2: potassium carbonate / N,N-dimethyl-formamide / 1 h / 50 - 60 °C

With sulfuric acid; sulfur trioxide; nitric acid; potassium carbonate; In N,N-dimethyl-formamide;
DOI:10.1016/j.bmc.2012.03.057