C₅H₁₃BrO₈P₂*C₁₆H₂₀N₂

Base Information

Chemical Name:C₅H₁₃BrO₈P₂*C₁₆H₂₀N₂
CAS No.:1399853-65-6
Molecular Formula:C₅H₁₃BrO₈P₂*C₁₆H₂₀N₂
Molecular Weight:583.353
Hs Code.:

C<sub>5</sub>H<sub>13</sub>BrO<sub>8</sub>P<sub>2</sub>*C<sub>16</sub>H<sub>20</sub>N<sub>2</sub>

Synonyms:C₅H₁₃BrO₈P₂*C₁₆H₂₀N₂

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Chemical Property of C₅H₁₃BrO₈P₂*C₁₆H₂₀N₂

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Technology Process of C₅H₁₃BrO₈P₂*C₁₆H₂₀N₂

There total 13 articles about C₅H₁₃BrO₈P₂*C₁₆H₂₀N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 756836-35-8
C₅H₁₃BrO₈P₂

: 140-28-3,87170-83-0
N,N'-Dibenzylethylenediamine

: 1399853-65-6
C₅H₁₃BrO₈P₂*C₁₆H₂₀N₂

Guidance literature:: In deuteromethanol;
DOI:10.1016/j.bmcl.2012.07.092

Reference yield:

: 169310-89-8
(2R)-4-(4-methoxyphenoxy)-2-methylbutane-1,2-diol

: 1399853-65-6
C₅H₁₃BrO₈P₂*C₁₆H₂₀N₂

Guidance literature:: Multi-step reaction with 10 steps

1.1: dmap; N-ethyl-N,N-diisopropylamine / chloroform / 3 h / Reflux; Inert atmosphere

2.1: ammonium cerium (IV) nitrate / water; acetonitrile / 0.5 h / 0 °C

3.1: dmap; N-ethyl-N,N-diisopropylamine / chloroform / 36 h / 20 °C / Inert atmosphere

4.1: caesium carbonate / acetone / 24 h / 20 °C

5.1: trimethylsilyl bromide; triphenylphosphine / dichloromethane / 0 - 20 °C

5.2: 1 h

6.1: pyridinium p-toluenesulfonate / dichloromethane / 3 h

7.1: acetonitrile / 18 h / 20 °C / Inert atmosphere

8.1: Dowex 50WX₈-100 (NH₄⁺ form)

9.1: Dowex 50WX₈-100 (H⁺ form)

10.1: deuteromethanol

With dmap; ammonium cerium (IV) nitrate; trimethylsilyl bromide; pyridinium p-toluenesulfonate; caesium carbonate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; In dichloromethane; deuteromethanol; chloroform; water; acetone; acetonitrile;
DOI:10.1016/j.bmcl.2012.07.092

Reference yield:

: 60299-29-8
(S)-(-)-2-Methylbutane-1,2,4-triol

: 1399853-65-6
C₅H₁₃BrO₈P₂*C₁₆H₂₀N₂

Guidance literature:: Multi-step reaction with 7 steps

1.1: tetra(n-butyl)ammonium hydrogensulfate; potassium hydroxide / dichloromethane / 3 h / 20 °C

2.1: trimethylsilyl bromide; triphenylphosphine / dichloromethane / 0 - 20 °C

2.2: 1 h

3.1: pyridinium p-toluenesulfonate / dichloromethane / 3 h

4.1: acetonitrile / 18 h / 20 °C / Inert atmosphere

5.1: Dowex 50WX₈-100 (NH₄⁺ form)

6.1: Dowex 50WX₈-100 (H⁺ form)

7.1: deuteromethanol

With trimethylsilyl bromide; tetra(n-butyl)ammonium hydrogensulfate; pyridinium p-toluenesulfonate; triphenylphosphine; potassium hydroxide; In dichloromethane; deuteromethanol; acetonitrile;
DOI:10.1016/j.bmcl.2012.07.092