nickel(II) 2,3,12,13-tetrabromo-5,10,15,20-tetra(4-isopropylphenyl)porphyrin

Base Information

• Chemical Name: nickel(II) 2,3,12,13-tetrabromo-5,10,15,20-tetra(4-isopropylphenyl)porphyrin
• CAS No.: 1189789-23-8
• Molecular Formula: C₅₆H₄₈Br₄N₄Ni
• Molecular Weight: 1155.33

Synonyms:nickel(II) 2,3,12,13-tetrabromo-5,10,15,20-tetra(4-isopropylphenyl)porphyrin

Chemical Property of nickel(II) 2,3,12,13-tetrabromo-5,10,15,20-tetra(4-isopropylphenyl)porphyrin

Chemical Property:

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Technology Process of nickel(II) 2,3,12,13-tetrabromo-5,10,15,20-tetra(4-isopropylphenyl)porphyrin

There total 1 articles about nickel(II) 2,3,12,13-tetrabromo-5,10,15,20-tetra(4-isopropylphenyl)porphyrin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

2,3,12,13-tetrabromo-5,10,15,20-tetra(4-isopropylphenyl)porphyrin → nickel(II) 2,3,12,13-tetrabromo-5,10,15,20-tetra(4-isopropylphenyl)porphyrin (1189789-23-8)

Guidance literature:

With nickel diacetate; In methanol; chloroform; Reflux;

DOI:10.1021/ol901615f

Reference yield: 53.0%

nickel(II) 2,3,12,13-tetrabromo-5,10,15,20-tetra(4-isopropylphenyl)porphyrin (1189789-23-8) + acrylic acid methyl ester (292638-85-8,9003-21-8,96-33-3) → C72H64N4NiO8 (1189789-25-0)

Guidance literature:

With palladium diacetate; potassium carbonate; triphenylphosphine; In N,N-dimethyl-formamide; toluene; for 72h; Inert atmosphere; Reflux;

DOI:10.1021/ol901615f

Reference yield: 48.0%

styrene (100-42-5,25038-60-2,25247-68-1,28213-80-1,28325-75-9,79637-11-9,9003-53-6) + nickel(II) 2,3,12,13-tetrabromo-5,10,15,20-tetra(4-isopropylphenyl)porphyrin (1189789-23-8) → C88H72N4Ni

Guidance literature:

With palladium diacetate; potassium carbonate; triphenylphosphine; In N,N-dimethyl-formamide; toluene; for 72h; Inert atmosphere; Reflux;

DOI:10.1021/ol901615f

Downstream raw materials:

C₇₂H₆₄N₄NiO₈

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