2,3',6-tris(benzyloxy)-4-<1-(carbo-tert-butoxy)-3,4-epoxybutoxy>-4'-propoxychalcone

Base Information

Chemical Name:2,3',6-tris(benzyloxy)-4-<1-(carbo-tert-butoxy)-3,4-epoxybutoxy>-4'-propoxychalcone
CAS No.:76799-46-7
Molecular Formula:C₄₈H₅₀O₉
Molecular Weight:770.92
Hs Code.:

Synonyms:2,3',6-tris(benzyloxy)-4-<1-(carbo-tert-butoxy)-3,4-epoxybutoxy>-4'-propoxychalcone

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Chemical Property of 2,3',6-tris(benzyloxy)-4-<1-(carbo-tert-butoxy)-3,4-epoxybutoxy>-4'-propoxychalcone

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Technology Process of 2,3',6-tris(benzyloxy)-4-<1-(carbo-tert-butoxy)-3,4-epoxybutoxy>-4'-propoxychalcone

There total 9 articles about 2,3',6-tris(benzyloxy)-4-<1-(carbo-tert-butoxy)-3,4-epoxybutoxy>-4'-propoxychalcone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 76799-42-3
tert-butyl 2-bromo-4,5-epoxypentanoate

: 76799-40-1
2,3',6-tris(benzyloxy)-4-hydroxy-4'-propoxychalcone

: 76799-46-7
2,3',6-tris(benzyloxy)-4-<1-(carbo-tert-butoxy)-3,4-epoxybutoxy>-4'-propoxychalcone

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; for 48h; Ambient temperature;
DOI:10.1021/jm00136a011

Reference yield:

: 10236-47-2
naringin

: 76799-46-7
2,3',6-tris(benzyloxy)-4-<1-(carbo-tert-butoxy)-3,4-epoxybutoxy>-4'-propoxychalcone

Guidance literature:: Multi-step reaction with 5 steps

1: 64 percent / 10percent aq. KOH / 4 h / Heating

2: 48.1 g / K₂CO₃ / dimethylformamide / 1.) RT, 21 h, 2.) 80 deg C, 6 h

3: 3.80 g / 3percent aq. H₂SO₄ / ethanol / 22 h

4: 76 percent / 60percent aq. KOH / ethanol / 72 h / Ambient temperature

5: 89 percent / K₂CO₃ / dimethylformamide / 48 h / Ambient temperature

With potassium hydroxide; sulfuric acid; potassium carbonate; In ethanol; N,N-dimethyl-formamide;
DOI:10.1021/jm00136a011

Reference yield:

: 39149-84-3
tert-butyl 2-bromo-4-pentenoate

: 76799-46-7
2,3',6-tris(benzyloxy)-4-<1-(carbo-tert-butoxy)-3,4-epoxybutoxy>-4'-propoxychalcone

Guidance literature:: Multi-step reaction with 2 steps

1: 59 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 14 h / Ambient temperature

2: 89 percent / K₂CO₃ / dimethylformamide / 48 h / Ambient temperature

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00136a011