N-(2-furylmethyl)-4-cyclohexylmethylsulfonyl-5-sulfamoyl-orthanilic acid phenyl ester

Base Information

Chemical Name:N-(2-furylmethyl)-4-cyclohexylmethylsulfonyl-5-sulfamoyl-orthanilic acid phenyl ester
CAS No.:79505-76-3
Molecular Formula:C₂₄H₂₈N₂O₈S₃
Molecular Weight:568.693
Hs Code.:

Synonyms:N-(2-furylmethyl)-4-cyclohexylmethylsulfonyl-5-sulfamoyl-orthanilic acid phenyl ester

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Chemical Property of N-(2-furylmethyl)-4-cyclohexylmethylsulfonyl-5-sulfamoyl-orthanilic acid phenyl ester

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Technology Process of N-(2-furylmethyl)-4-cyclohexylmethylsulfonyl-5-sulfamoyl-orthanilic acid phenyl ester

There total 7 articles about N-(2-furylmethyl)-4-cyclohexylmethylsulfonyl-5-sulfamoyl-orthanilic acid phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4-Cyclohexylmethylsulfanyl-2-[(furan-2-ylmethyl)-amino]-5-sulfamoyl-benzenesulfonic acid phenyl ester

: 79505-76-3
N-(2-furylmethyl)-4-cyclohexylmethylsulfonyl-5-sulfamoyl-orthanilic acid phenyl ester

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; for 3h; Ambient temperature;
DOI:10.1021/jm00362a017

Reference yield:

: 617-89-0
furan-2-ylmethanamine

: 79505-76-3
N-(2-furylmethyl)-4-cyclohexylmethylsulfonyl-5-sulfamoyl-orthanilic acid phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 1.5 h / 90 °C

2: 85percent 3-chloroperbenzoic acid / CH₂Cl₂ / 3 h / Ambient temperature

With 3-chloro-benzenecarboperoxoic acid; In dichloromethane;
DOI:10.1021/jm00362a017

Reference yield:

: 61791-73-9
4,6-dichlorobenzene-1,3-disulfonyl chloride

: 79505-76-3
N-(2-furylmethyl)-4-cyclohexylmethylsulfonyl-5-sulfamoyl-orthanilic acid phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 1.) NH₃ / 1.) THF, 5-10 deg C, 2 h, 2.) MeOH, a) reflux, 10 min, b) RT, overnight

2: K₂CO₃ / dimethylformamide / 1 h / 115 °C

3: 1.5 h / 90 °C

4: 85percent 3-chloroperbenzoic acid / CH₂Cl₂ / 3 h / Ambient temperature

With ammonia; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/jm00362a017