1H-pyrido<3,4,5-de>quinazoline

Base Information

• Chemical Name: 1H-pyrido<3,4,5-de>quinazoline
• CAS No.: 110748-36-2
• Molecular Formula: C₁₀H₇N₃
• Molecular Weight: 169.186

Synonyms:1H-pyrido<3,4,5-de>quinazoline

Chemical Property of 1H-pyrido<3,4,5-de>quinazoline

Chemical Property:

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Technology Process of 1H-pyrido<3,4,5-de>quinazoline

There total 1 articles about 1H-pyrido<3,4,5-de>quinazoline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-nitro-isoquinoline (36073-93-5) → 1H-pyrido<3,4,5-de>quinazoline (110748-36-2)

Guidance literature:

Multi-step reaction with 3 steps

1: 73 percent / potassium nitrate, conc. H₂SO₄ / 2.5 h / 75 °C

2: 94 percent / H₂ / 10percent Pd/C / acetic acid / 1 h / 2068.6 Torr / Ambient temperature

3: 73 percent / 0.5 h / Heating

With sulfuric acid; hydrogen; potassium nitrate; palladium on activated charcoal; In acetic acid;

upstream raw materials:

4-nitro-isoquinoline

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