C₃₃H₄₀Cl₄O₆Si

Base Information

Chemical Name:C₃₃H₄₀Cl₄O₆Si
CAS No.:1027966-29-5
Molecular Formula:C₃₃H₄₀Cl₄O₆Si
Molecular Weight:702.575
Hs Code.:

C<sub>33</sub>H<sub>40</sub>Cl<sub>4</sub>O<sub>6</sub>Si

Synonyms:C₃₃H₄₀Cl₄O₆Si

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Chemical Property of C₃₃H₄₀Cl₄O₆Si

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Technology Process of C₃₃H₄₀Cl₄O₆Si

There total 10 articles about C₃₃H₄₀Cl₄O₆Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₂₈H₃₂Cl₄O₄

: 1027966-29-5
C₃₃H₄₀Cl₄O₆Si

Guidance literature:: Multi-step reaction with 9 steps

1: (PCy₃)2Ru=CHPh / CH₂Cl₂ / 5 h / Heating

2: 3.50 g / lead(IV) acetate / CH₂Cl₂ / 20 °C

3: 53 percent / (-)-N-(1-phenylethyl)-1-azabicyclo[2.2.2]octan-3-amine; lithium chloride; n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C

4: m-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / 20 °C

5: florisil / CH₂Cl₂ / 2 h

6: 4.90 g / IBX / dimethylsulfoxide / 1 h / 20 °C

7: 4.36 g / N,N-dimethylaniline / CH₂Cl₂ / -78 - 20 °C

8: 73 percent / tributyltin hydride; BEt₃; air / toluene; hexane / 0.5 h / 20 °C

9: N,N-diisopropylethylamine / CH₂Cl₂ / 4 h / -20 °C

With lead(IV) acetate; florisil; n-butyllithium; air; triethyl borane; tri-n-butyl-tin hydride; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; (PCy₃)2Ru=CHPh; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jo0700474

Reference yield:

: C₂₆H₂₆Cl₄O₄

: 1027966-29-5
C₃₃H₄₀Cl₄O₆Si

Guidance literature:: Multi-step reaction with 7 steps

1: 53 percent / (-)-N-(1-phenylethyl)-1-azabicyclo[2.2.2]octan-3-amine; lithium chloride; n-butyllithium / tetrahydrofuran; hexane / 0.17 h / -78 °C

2: m-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / 20 °C

3: florisil / CH₂Cl₂ / 2 h

4: 4.90 g / IBX / dimethylsulfoxide / 1 h / 20 °C

5: 4.36 g / N,N-dimethylaniline / CH₂Cl₂ / -78 - 20 °C

6: 73 percent / tributyltin hydride; BEt₃; air / toluene; hexane / 0.5 h / 20 °C

7: N,N-diisopropylethylamine / CH₂Cl₂ / 4 h / -20 °C

With florisil; n-butyllithium; air; triethyl borane; tri-n-butyl-tin hydride; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; lithium chloride; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In tetrahydrofuran; hexane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jo0700474

Reference yield:

: 936338-30-6
C₂₆H₂₆Cl₄O₄

: 1027966-29-5
C₃₃H₄₀Cl₄O₆Si

Guidance literature:: Multi-step reaction with 6 steps

1: m-chloroperoxybenzoic acid / CH₂Cl₂ / 4 h / 20 °C

2: florisil / CH₂Cl₂ / 2 h

3: 4.90 g / IBX / dimethylsulfoxide / 1 h / 20 °C

4: 4.36 g / N,N-dimethylaniline / CH₂Cl₂ / -78 - 20 °C

5: 73 percent / tributyltin hydride; BEt₃; air / toluene; hexane / 0.5 h / 20 °C

6: N,N-diisopropylethylamine / CH₂Cl₂ / 4 h / -20 °C

With florisil; air; triethyl borane; tri-n-butyl-tin hydride; N,N-dimethyl-aniline; N-ethyl-N,N-diisopropylamine; 3-chloro-benzenecarboperoxoic acid; 1-hydroxy-3H-benz[d][1,2]iodoxole-1,3-dione; In hexane; dichloromethane; dimethyl sulfoxide; toluene;
DOI:10.1021/jo0700474