1,3-Diazidobenzene

Base Information

Chemical Name:1,3-Diazidobenzene
CAS No.:13556-50-8
Molecular Formula:C₆H₄N₆
Molecular Weight:160.138
Hs Code.:
DSSTox Substance ID:DTXSID40561827
Nikkaji Number:J1.450.344G
Wikidata:Q82445711
Mol file:13556-50-8.mol

Synonyms:1,3-diazidobenzene;13556-50-8;SCHEMBL16748956;XNRIPCDSMGRSPE-UHFFFAOYSA-;DTXSID40561827;InChI=1/C6H4N6/c7-11-9-5-2-1-3-6(4-5)10-12-8/h1-4H

Suppliers and Price of 1,3-Diazidobenzene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 5 raw suppliers

Chemical Property of 1,3-Diazidobenzene

Chemical Property:

Refractive Index:1.8300 (estimate)
Boiling Point:276.02°C (rough estimate)
PSA：99.50000
Density:1.4978 (rough estimate)
LogP:2.47572
XLogP3:3.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:2
Exact Mass:160.04974415
Heavy Atom Count:12
Complexity:212

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s): 3
Hazard Codes:3

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC(=CC(=C1)N=[N+]=[N-])N=[N+]=[N-]

Technology Process of 1,3-Diazidobenzene

There total 2 articles about 1,3-Diazidobenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 108-45-2,64554-26-3,76583-20-5
m-phenylenediamine

: 13556-50-8
n-phenylenediazide

Guidance literature:: m-phenylenediamine; With sulfuric acid; sodium nitrite; In water; at 0 - 2 ℃;

With sodium azide; In water; at 0 - 5 ℃;
DOI:10.1246/bcsj.76.2075

Reference yield:

: 615-28-1
o-phenylenediamine dihydrochloride

: 13556-50-8
n-phenylenediazide

Guidance literature:: With sulfuric acid; man fuegt Natriumazid hinzu, diazotiert mit Natriumnitrit und setzt weiter Natriumazid hinzu;

Reference yield: 80.0%

: 13556-50-8
n-phenylenediazide

: 4-(2-hydroxyphenyl)-1-(prop-2-yn-1-yl)-1,5-benzodiazepin-2-one

: 1,1'-((1,1'-(1,3-phenylene)bis(1H-1,2,3-triazole-4,1-diyl))bis(methylene))bis(1,5-benzodiazepin-2-one)

Guidance literature:: With copper(l) iodide; N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; for 0.133333h; regioselective reaction; Microwave irradiation;
DOI:10.1016/j.molstruc.2019.06.018