(E)-1-(3-chloro-4-methyl-1-phenylpentan-3-yl)-2-(4-chlorophenyl)diazene

Base Information

Chemical Name:(E)-1-(3-chloro-4-methyl-1-phenylpentan-3-yl)-2-(4-chlorophenyl)diazene
CAS No.:1381772-60-6
Molecular Formula:C₁₈H₂₀Cl₂N₂
Molecular Weight:335.276
Hs Code.:

Synonyms:(E)-1-(3-chloro-4-methyl-1-phenylpentan-3-yl)-2-(4-chlorophenyl)diazene

Suppliers and Price of (E)-1-(3-chloro-4-methyl-1-phenylpentan-3-yl)-2-(4-chlorophenyl)diazene

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Total 1 raw suppliers

Chemical Property of (E)-1-(3-chloro-4-methyl-1-phenylpentan-3-yl)-2-(4-chlorophenyl)diazene

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
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Technology Process of (E)-1-(3-chloro-4-methyl-1-phenylpentan-3-yl)-2-(4-chlorophenyl)diazene

There total 3 articles about (E)-1-(3-chloro-4-methyl-1-phenylpentan-3-yl)-2-(4-chlorophenyl)diazene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1381772-21-9
(Z)-1-(4-chlorophenyl)-2-(4-methyl-1-phenylpentan-3-ylidene)hydrazine

: 1381772-60-6
(E)-1-(3-chloro-4-methyl-1-phenylpentan-3-yl)-2-(4-chlorophenyl)diazene

Guidance literature:: (Z)-1-(4-chlorophenyl)-2-(4-methyl-1-phenylpentan-3-ylidene)hydrazine; With oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; at -78 - -55 ℃; for 0.166667h; Inert atmosphere;

With triethylamine; In tetrahydrofuran; at 25 ℃; for 0.0833333h; Inert atmosphere;
DOI:10.1021/ja303054c

Reference yield:

: 3277-89-2
phenethylmagnesium bromide

: 1381772-60-6
(E)-1-(3-chloro-4-methyl-1-phenylpentan-3-yl)-2-(4-chlorophenyl)diazene

Guidance literature:: Multi-step reaction with 3 steps

1.1: copper(l) iodide / Inert atmosphere

2.1: dichloromethane / 17 h / Molecular sieve; Inert atmosphere; Reflux

3.1: oxalyl dichloride; dimethyl sulfoxide / tetrahydrofuran / 0.17 h / -78 - -55 °C / Inert atmosphere

3.2: 0.08 h / 25 °C / Inert atmosphere

With copper(l) iodide; oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane; 1.1: Grignard reaction;
DOI:10.1021/ja303054c

Reference yield:

: 1073-69-4
N-4-chlorophenylhydrazine

: 1381772-60-6
(E)-1-(3-chloro-4-methyl-1-phenylpentan-3-yl)-2-(4-chlorophenyl)diazene

Guidance literature:: Multi-step reaction with 2 steps

1.1: dichloromethane / 17 h / Molecular sieve; Inert atmosphere; Reflux

2.1: oxalyl dichloride; dimethyl sulfoxide / tetrahydrofuran / 0.17 h / -78 - -55 °C / Inert atmosphere

2.2: 0.08 h / 25 °C / Inert atmosphere

With oxalyl dichloride; dimethyl sulfoxide; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja303054c