(1R,3R)-2-Benzyl-1-[1,3]dithian-2-ylmethyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester

Base Information

• Chemical Name: (1R,3R)-2-Benzyl-1-[1,3]dithian-2-ylmethyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester
• CAS No.: 185419-04-9
• Molecular Formula: C₂₅H₂₈N₂O₂S₂
• Molecular Weight: 452.642

Synonyms:(1R,3R)-2-Benzyl-1-[1,3]dithian-2-ylmethyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester

Chemical Property of (1R,3R)-2-Benzyl-1-[1,3]dithian-2-ylmethyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester

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Technology Process of (1R,3R)-2-Benzyl-1-[1,3]dithian-2-ylmethyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester

There total 1 articles about (1R,3R)-2-Benzyl-1-[1,3]dithian-2-ylmethyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-(+)-Nbbenzyltryptophan methyl ester (63229-68-5,73327-10-3,84094-71-3) + [1,3]dithian-2-yl-acetaldehyde (57688-55-8) → (1S,3R)-2-Benzyl-1-[1,3]dithian-2-ylmethyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester + (1R,3R)-2-Benzyl-1-[1,3]dithian-2-ylmethyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester (185419-04-9)

Guidance literature:

In benzene; Yield given. Yields of byproduct given; Heating;

DOI:10.1039/CC9960002477

Reference yield: 94.0%

(1R,3R)-2-Benzyl-1-[1,3]dithian-2-ylmethyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester (185419-04-9) → (1S,3R)-2-Benzyl-1-[1,3]dithian-2-ylmethyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester

Guidance literature:

With trifluoroacetic acid; In dichloromethane; Ambient temperature;

DOI:10.1039/CC9960002477

Reference yield: 25.0%

(1R,3R)-2-Benzyl-1-[1,3]dithian-2-ylmethyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester (185419-04-9) → (R)-2-Benzylamino-3-[2-(2-[1,3]dithian-2-yl-ethyl)-1H-indol-3-yl]-propionic acid methyl ester + (1S,3R)-2-Benzyl-1-[1,3]dithian-2-ylmethyl-2,3,4,9-tetrahydro-1H-β-carboline-3-carboxylic acid methyl ester

Guidance literature:

With sodium tetrahydroborate; trifluoroacetic acid; In dichloromethane; for 17.5h; Ambient temperature;

DOI:10.1021/jo951170a

upstream raw materials:

D-(+)-N_bbenzyltryptophan methyl ester

[1,3]dithian-2-yl-acetaldehyde

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