C₂₅H₃₂O₄

Base Information

Chemical Name:C₂₅H₃₂O₄
CAS No.:947253-37-4
Molecular Formula:C₂₅H₃₂O₄
Molecular Weight:396.527
Hs Code.:

C<sub>25</sub>H<sub>32</sub>O<sub>4</sub>

Synonyms:C₂₅H₃₂O₄

Suppliers and Price of C₂₅H₃₂O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₅H₃₂O₄

Chemical Property:

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Technology Process of C₂₅H₃₂O₄

There total 7 articles about C₂₅H₃₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

: 947253-62-5
C₂₈H₃₈O₃Si

: 947253-37-4
C₂₅H₃₂O₄

Guidance literature:: With sulfuric acid; mercury(II) oxide; In acetone; at 50 ℃; for 1h;
DOI:10.1055/s-2007-982556

Reference yield:

: 947253-54-5
C₂₃H₂₈O₄

: 947253-37-4
C₂₅H₃₂O₄

Guidance literature:: Multi-step reaction with 4 steps

1: 95 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 12 h / 20 °C

2: 90 percent / n-BuLi / tetrahydrofuran / 1.5 h / -78 °C

3: 85 percent / triethyl silane; boron trifluoride*diethyl ether / CH₂Cl₂; acetonitrile / 2 h / -40 °C

4: 70 percent / mercury(II) oxide; aqueous sulfuric acid / acetone / 1 h / 50 °C

With triethylsilane; n-butyllithium; sulfuric acid; boron trifluoride diethyl etherate; 1,8-diazabicyclo[5.4.0]undec-7-ene; mercury(II) oxide; In tetrahydrofuran; dichloromethane; acetone; acetonitrile;
DOI:10.1055/s-2007-982556

Reference yield:

: 947253-52-3
C₂₃H₃₀O₄

: 947253-37-4
C₂₅H₃₂O₄

Guidance literature:: Multi-step reaction with 5 steps

1: 100 percent / pyridinium chlorochromate; NaOAc / 3 h / 20 °C

2: 95 percent / 1,8-diazabicyclo[5.4.0]undec-7-ene / tetrahydrofuran / 12 h / 20 °C

3: 90 percent / n-BuLi / tetrahydrofuran / 1.5 h / -78 °C

4: 85 percent / triethyl silane; boron trifluoride*diethyl ether / CH₂Cl₂; acetonitrile / 2 h / -40 °C

5: 70 percent / mercury(II) oxide; aqueous sulfuric acid / acetone / 1 h / 50 °C

With triethylsilane; n-butyllithium; sulfuric acid; boron trifluoride diethyl etherate; sodium acetate; 1,8-diazabicyclo[5.4.0]undec-7-ene; pyridinium chlorochromate; mercury(II) oxide; In tetrahydrofuran; dichloromethane; acetone; acetonitrile;
DOI:10.1055/s-2007-982556