methyl 5-(N-(4-heptylbenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoic acid

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Chemical Name:methyl 5-(N-(4-heptylbenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoic acid
CAS No.:1456601-85-6
Molecular Formula:C₃₇H₄₂N₂O₆S
Molecular Weight:642.816
Hs Code.:

Synonyms:methyl 5-(N-(4-heptylbenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoic acid

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Chemical Property of methyl 5-(N-(4-heptylbenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoic acid

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Technology Process of methyl 5-(N-(4-heptylbenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoic acid

There total 6 articles about methyl 5-(N-(4-heptylbenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 1456601-64-1
methyl 5-(4-heptylbenzylamino)-2-hydroxybenzoate

: 381193-32-4
2-(N-methylbiphenyl-4-ylsulfonamido)acetic acid

: 1456601-85-6
methyl 5-(N-(4-heptylbenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoic acid

Guidance literature:: With dichlorotriphenylphosphorane; In dichloromethane; at 80 ℃; for 1h; Inert atmosphere; Microwave irradiation;
DOI:10.1039/c3md20323a

Reference yield: 50.0%

: 1456601-85-6
methyl 5-(N-(4-heptylbenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoic acid

Guidance literature:: With dichlorotriphenylphosphorane; In dichloromethane; at 80 ℃; for 1h; Inert atmosphere; Microwave irradiation;

Reference yield:

: 42753-75-3
methyl 5-amino-2-hydroxybenzoate

: 1456601-85-6
methyl 5-(N-(4-heptylbenzyl)-2-(N-methylbiphenyl-4-ylsulfonamido)acetamido)-2-hydroxybenzoic acid

Guidance literature:: Multi-step reaction with 2 steps

1.1: acetic acid / methanol / 1 h / 20 - 40 °C / Molecular sieve

1.2: 2 h / 5 - 20 °C

2.1: dichlorotriphenylphosphorane / dichloromethane / 1 h / 80 °C / Inert atmosphere; Microwave irradiation

With acetic acid; dichlorotriphenylphosphorane; In methanol; dichloromethane;
DOI:10.1039/c3md20323a