2-(2-ethylsulfanylphenyl)-6-(3-fluorophenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

Base Information

Chemical Name:2-(2-ethylsulfanylphenyl)-6-(3-fluorophenyl)-3-methyl-3H-imidazo[4,5-b]pyridine
CAS No.:1383944-75-9
Molecular Formula:C₂₁H₁₈FN₃S
Molecular Weight:363.458
Hs Code.:

Synonyms:2-(2-ethylsulfanylphenyl)-6-(3-fluorophenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

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Chemical Property of 2-(2-ethylsulfanylphenyl)-6-(3-fluorophenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

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Technology Process of 2-(2-ethylsulfanylphenyl)-6-(3-fluorophenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

There total 3 articles about 2-(2-ethylsulfanylphenyl)-6-(3-fluorophenyl)-3-methyl-3H-imidazo[4,5-b]pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1383944-56-6
6-bromo-2-(2-ethyl-sulfanyl-phenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

: 768-35-4
3-fluorophenylboronic acid

: 1383944-75-9
2-(2-ethylsulfanylphenyl)-6-(3-fluorophenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

Guidance literature:: With sodium carbonate; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In 1,4-dioxane; at 80 ℃; for 8h;

Reference yield:

: 21101-79-1
2-ethylsulfanylbenzoic acid

: 1383944-75-9
2-(2-ethylsulfanylphenyl)-6-(3-fluorophenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / 0.5 h / 120 °C

1.2: 1 h / 140 °C

2.1: sodium carbonate / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / 1,4-dioxane / 8 h / 80 °C

With sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In 1,4-dioxane;

Reference yield:

: 89415-54-3
5-bromo-N²-methylpyridine-2,3-diamine

: 1383944-75-9
2-(2-ethylsulfanylphenyl)-6-(3-fluorophenyl)-3-methyl-3H-imidazo[4,5-b]pyridine

Guidance literature:: Multi-step reaction with 2 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / 0.5 h / 120 °C

1.2: 1 h / 140 °C

2.1: sodium carbonate / palladium bis[bis(diphenylphosphino)ferrocene] dichloride / 1,4-dioxane / 8 h / 80 °C

With sodium carbonate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium bis[bis(diphenylphosphino)ferrocene] dichloride; In 1,4-dioxane;