Benzyl-7-O-(tert-butyldiphenylsilyl)-L-glycero-α-D-manno-heptofuranosid

Base Information

Chemical Name:Benzyl-7-O-(tert-butyldiphenylsilyl)-L-glycero-α-D-manno-heptofuranosid
CAS No.:116265-17-9
Molecular Formula:C₃₀H₃₈O₇Si
Molecular Weight:538.713
Hs Code.:

Synonyms:Benzyl-7-O-(tert-butyldiphenylsilyl)-L-glycero-α-D-manno-heptofuranosid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Benzyl-7-O-(tert-butyldiphenylsilyl)-L-glycero-α-D-manno-heptofuranosid

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Technology Process of Benzyl-7-O-(tert-butyldiphenylsilyl)-L-glycero-α-D-manno-heptofuranosid

There total 3 articles about Benzyl-7-O-(tert-butyldiphenylsilyl)-L-glycero-α-D-manno-heptofuranosid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 116265-16-8
(1R,2S)-1-((2R,3R,4S,5S)-5-Benzyloxy-3,4-dihydroxy-tetrahydro-furan-2-yl)-propane-1,2,3-triol

: 58479-61-1
tert-butylchlorodiphenylsilane

: 116265-17-9
Benzyl-7-O-(tert-butyldiphenylsilyl)-L-glycero-α-D-manno-heptofuranosid

Guidance literature:: With 1H-imidazole; In N,N-dimethyl-formamide; at 0 ℃; for 5h; Yield given;

Reference yield:

: 116265-15-7
Benzyl-5,6,7-tri-O-acetyl-L-glycero-α-D-manno-heptofuranosid

: 116265-17-9
Benzyl-7-O-(tert-butyldiphenylsilyl)-L-glycero-α-D-manno-heptofuranosid

Guidance literature:: Multi-step reaction with 2 steps

1: 0.7 g / 1N CH₃ONa / methanol / 0.5 h / Ambient temperature

2: imidazole / dimethylformamide / 5 h / 0 °C

With 1H-imidazole; sodium methylate; In methanol; N,N-dimethyl-formamide;

Reference yield:

: 105592-31-2
benzyl 5,6,7-tri-O-acetyl-2,3-O-isopropylidene-β-L-glycero-D-manno-heptofuranoside

: 116265-17-9
Benzyl-7-O-(tert-butyldiphenylsilyl)-L-glycero-α-D-manno-heptofuranosid

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / CF₃CO₂H / CH₂Cl₂; H₂O / 1.5 h / Ambient temperature

2: 0.7 g / 1N CH₃ONa / methanol / 0.5 h / Ambient temperature

3: imidazole / dimethylformamide / 5 h / 0 °C

With 1H-imidazole; sodium methylate; trifluoroacetic acid; In methanol; dichloromethane; water; N,N-dimethyl-formamide;