(2Z)-2-Amino-3-{[(1E)-(2-hydroxyphenyl)methylidene]-amino}but-2-enedinitrile

Base Information

• Chemical Name: (2Z)-2-Amino-3-{[(1E)-(2-hydroxyphenyl)methylidene]-amino}but-2-enedinitrile
• CAS No.: 946529-82-4
• Molecular Formula: C₁₁H₈N₄O
• Molecular Weight: 212.211
• Mol file: 946529-82-4.mol

Synonyms:(2Z)-2-Amino-3-{[(1E)-(2-hydroxyphenyl)methylidene]-amino}but-2-enedinitrile

Chemical Property of (2Z)-2-Amino-3-{[(1E)-(2-hydroxyphenyl)methylidene]-amino}but-2-enedinitrile

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (2Z)-2-Amino-3-{[(1E)-(2-hydroxyphenyl)methylidene]-amino}but-2-enedinitrile

There total 2 articles about (2Z)-2-Amino-3-{[(1E)-(2-hydroxyphenyl)methylidene]-amino}but-2-enedinitrile which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

salicylaldehyde (90-02-8) + diaminomaleonitrile (1187-42-4) → (2Z)-2-Amino-3-{[(1E)-(2-hydroxyphenyl)methylidene]-amino}but-2-enedinitrile (946529-82-4)

Guidance literature:

In methanol; for 2h; Reflux;

DOI:10.1016/j.ica.2015.11.026

Reference yield: 49.2%

2-methyl-benzyl alcohol (89-95-2) + diaminomaleonitrile (1187-42-4) → (2Z)-2-Amino-3-{[(1E)-(2-hydroxyphenyl)methylidene]-amino}but-2-enedinitrile (946529-82-4)

Guidance literature:

In water; at 20 ℃;

DOI:10.3390/11110858

upstream raw materials:

2-methyl-benzyl alcohol

diaminomaleonitrile

salicylaldehyde