C₁₆H₂₆O₃

Base Information

Chemical Name:C₁₆H₂₆O₃
CAS No.:1123785-74-9
Molecular Formula:C₁₆H₂₆O₃
Molecular Weight:266.381
Hs Code.:

C<sub>16</sub>H<sub>26</sub>O<sub>3</sub>

Synonyms:C₁₆H₂₆O₃

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Chemical Property of C₁₆H₂₆O₃

Chemical Property:

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Technology Process of C₁₆H₂₆O₃

There total 6 articles about C₁₆H₂₆O₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1123785-11-4
(2R,3R,6S)-7-(benzyloxy)-3-(tert-butyldimethylsilyloxy)-2,6-dimethylheptan-1-ol

: 1123785-74-9
C₁₆H₂₆O₃

Guidance literature:: With tetrabutyl ammonium fluoride; In tetrahydrofuran; at 20 ℃; for 1h;
DOI:10.1016/j.tetlet.2008.11.088

Reference yield:

: 887706-39-0
(S)-5-(benzyloxy)-4-methylpentan-1-ol

: 1123785-74-9
C₁₆H₂₆O₃

Guidance literature:: Multi-step reaction with 5 steps

1.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

2.1: di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 0.17 h / 0 °C

2.2: 0.5 h / 0 °C

2.3: 1 h / 0 °C

3.1: 2,6-dimethylpyridine / 0.5 h / 0 °C

4.1: sodium tetrahydroborate; lithium chloride / tetrahydrofuran; ethanol / 6 h / 20 °C

5.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C

With 2,6-dimethylpyridine; sodium tetrahydroborate; di-n-butylboryl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; Dess-Martin periodane; lithium chloride; In tetrahydrofuran; ethanol; dichloromethane; 2.1: |Evans Aldol Reaction / 2.2: |Evans Aldol Reaction;
DOI:10.1016/j.tetasy.2012.07.006

Reference yield:

: 391208-05-2
(S)-1-((2-methylpent-4-enyloxy)methyl)benzene

: 1123785-74-9
C₁₆H₂₆O₃

Guidance literature:: Multi-step reaction with 6 steps

1.1: dimethylsulfide borane complex / tetrahydrofuran / 5 h / 0 °C

1.2: 16 h / 20 °C

2.1: Dess-Martin periodane / dichloromethane / 1 h / 20 °C

3.1: di-n-butylboryl trifluoromethanesulfonate / dichloromethane / 0.17 h / 0 °C

3.2: 0.5 h / 0 °C

3.3: 1 h / 0 °C

4.1: 2,6-dimethylpyridine / 0.5 h / 0 °C

5.1: sodium tetrahydroborate; lithium chloride / tetrahydrofuran; ethanol / 6 h / 20 °C

6.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 0.5 h / 0 °C

With 2,6-dimethylpyridine; sodium tetrahydroborate; dimethylsulfide borane complex; di-n-butylboryl trifluoromethanesulfonate; tetrabutyl ammonium fluoride; Dess-Martin periodane; lithium chloride; In tetrahydrofuran; ethanol; dichloromethane; 3.1: |Evans Aldol Reaction / 3.2: |Evans Aldol Reaction;
DOI:10.1016/j.tetasy.2012.07.006