1,3-dimesityl-2-(2',3',4',5'-tetraethylphospholyl)tetrahydro-1,3,2-diazaphosphole

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Chemical Name:1,3-dimesityl-2-(2',3',4',5'-tetraethylphospholyl)tetrahydro-1,3,2-diazaphosphole
CAS No.:1127351-54-5
Molecular Formula:C₃₀H₄₀N₂P₂
Molecular Weight:490.609
Hs Code.:

Synonyms:1,3-dimesityl-2-(2',3',4',5'-tetraethylphospholyl)tetrahydro-1,3,2-diazaphosphole

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Chemical Property of 1,3-dimesityl-2-(2',3',4',5'-tetraethylphospholyl)tetrahydro-1,3,2-diazaphosphole

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Technology Process of 1,3-dimesityl-2-(2',3',4',5'-tetraethylphospholyl)tetrahydro-1,3,2-diazaphosphole

There total 1 articles about 1,3-dimesityl-2-(2',3',4',5'-tetraethylphospholyl)tetrahydro-1,3,2-diazaphosphole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 312920-30-2
1-chloro-2,3,4,5-tetraethylphosphole

: 905994-37-8
1,3-bis(2,6-dimethylphenyl)-2-chloro-dihydro-1,3,2-diazaphosphole

: 1127351-54-5
1,3-dimesityl-2-(2',3',4',5'-tetraethylphospholyl)tetrahydro-1,3,2-diazaphosphole

Guidance literature:: 1-chloro-2,3,4,5-tetraethylphosphole; With lithium; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

1,3-bis(2,6-dimethylphenyl)-2-chloro-dihydro-1,3,2-diazaphosphole; In tetrahydrofuran; at -78 - 20 ℃; Inert atmosphere;
DOI:10.1021/ja903156p

Reference yield: 81.0%

: η5-cyclopentadienylbis(ethene)cobalt

: 1127351-54-5
1,3-dimesityl-2-(2',3',4',5'-tetraethylphospholyl)tetrahydro-1,3,2-diazaphosphole

: (η1-cyclopentadienyl)(η1-1,3-bis(2',6'-dimethylphenyl)-2,3-dihydro-1,3,2-diazaphospholyl)(η5-2',3',4',5'-tetraethylphospholyl)cobalt(I)

Guidance literature:: In tetrahydrofuran; byproducts: C2H4; (Ar); vac. technique; soln. of P compd. and Co complex in THF was stirred for 1 h; evapd. (vac.); dissolved in pentane; kept at -20°C; filtered; dried (vac.); elem. anal.;
DOI:10.1021/om801008s