19-glutaramide-2,7,12,17-tetraphenylporphycene

Base Information

• Chemical Name: 19-glutaramide-2,7,12,17-tetraphenylporphycene
• CAS No.: 1417886-16-8
• Molecular Formula: C₄₉H₃₇N₅O₃
• Molecular Weight: 743.864
• Mol file: 1417886-16-8.mol

Synonyms:19-glutaramide-2,7,12,17-tetraphenylporphycene

Chemical Property of 19-glutaramide-2,7,12,17-tetraphenylporphycene

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 19-glutaramide-2,7,12,17-tetraphenylporphycene

There total 4 articles about 19-glutaramide-2,7,12,17-tetraphenylporphycene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 70.0%

9-(glutaric methylesteramide)-2,7,12,17-tetraphenylporphycene (1358543-19-7) → 19-glutaramide-2,7,12,17-tetraphenylporphycene (1417886-16-8)

Guidance literature:

With water; sodium hydroxide; In tetrahydrofuran; methanol; at 20 ℃; for 0.833333h;

DOI:10.1021/jm301509n

Reference yield:

9-nitro-2,7,12,17-tetraphenylporphycene (1358543-12-0) → 19-glutaramide-2,7,12,17-tetraphenylporphycene (1417886-16-8)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium dithionite / dichloromethane

With sodium dithionite; In dichloromethane;

DOI:10.1142/S1088424619500986

Reference yield:

2,7,12,17-tetraphenylporphycene (164414-55-5) → 19-glutaramide-2,7,12,17-tetraphenylporphycene (1417886-16-8)

Guidance literature:

Multi-step reaction with 3 steps

1: silver nitrate / acetic acid

2: sodium dithionite / dichloromethane

With sodium dithionite; silver nitrate; In dichloromethane; acetic acid;

DOI:10.1142/S1088424619500986

upstream raw materials:

9-(glutaric methylesteramide)-2,7,12,17-tetraphenylporphycene

methyl 4-(chlorocarbonyl)butyrate

9-nitro-2,7,12,17-tetraphenylporphycene

2,7,12,17-tetraphenylporphycene