Cyclododecyl (2,4-dimethoxybenzoyl)formate

Base Information

• Chemical Name: Cyclododecyl (2,4-dimethoxybenzoyl)formate
• CAS No.: 164167-33-3
• Molecular Formula: C₂₂H₃₂O₅
• Molecular Weight: 376.493
• Mol file: 164167-33-3.mol

Synonyms:Cyclododecyl (2,4-dimethoxybenzoyl)formate

Chemical Property of Cyclododecyl (2,4-dimethoxybenzoyl)formate

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of Cyclododecyl (2,4-dimethoxybenzoyl)formate

There total 1 articles about Cyclododecyl (2,4-dimethoxybenzoyl)formate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

cyclododecanol (1724-39-6) + 2-(2,4-dimethoxybenzene)-2-oxoacetic acid (26767-17-9) → Cyclododecyl (2,4-dimethoxybenzoyl)formate (164167-33-3)

Guidance literature:

With sodium ethanolate; 1,1'-carbonyldiimidazole; In tetrahydrofuran; 1.) 30 min, 2.) 25 h;

DOI:10.1021/jo00113a029

Reference yield:

isopropyl alcohol (67-63-0,8013-70-5) + Cyclododecyl (2,4-dimethoxybenzoyl)formate (164167-33-3) → cyclododecanone (830-13-7) + 2,4-Dimethoxybenzaldehyde (613-45-6) + Isopropyl 2,4-dimethoxymandelate

Guidance literature:

In benzene; for 1h; Yields of byproduct given; Irradiation;

DOI:10.1021/jo00113a029

Reference yield:

Cyclododecyl (2,4-dimethoxybenzoyl)formate (164167-33-3) → cyclododecanone (830-13-7) + 2,4-Dimethoxybenzaldehyde (613-45-6)

Guidance literature:

In acetonitrile; for 8h; Yield given. Yields of byproduct given; Irradiation;

DOI:10.1021/jo00113a029

upstream raw materials:

cyclododecanol

2-(2,4-dimethoxybenzene)-2-oxoacetic acid

Downstream raw materials:

cyclododecanone

2,4-Dimethoxybenzaldehyde