4-(1,3-Dioxo-1,3,3a,4,7,7a-hexahydro-isoindol-2-yl)-3-oxo-N-phenyl-2-(triphenyl-λ⁵-phosphanylidene)-butyramide

Base Information

• Chemical Name: 4-(1,3-Dioxo-1,3,3a,4,7,7a-hexahydro-isoindol-2-yl)-3-oxo-N-phenyl-2-(triphenyl-λ⁵-phosphanylidene)-butyramide
• CAS No.: 108159-78-0
• Molecular Formula: C₃₆H₃₁N₂O₄P
• Molecular Weight: 586.627

Synonyms:4-(1,3-Dioxo-1,3,3a,4,7,7a-hexahydro-isoindol-2-yl)-3-oxo-N-phenyl-2-(triphenyl-λ⁵-phosphanylidene)-butyramide

Chemical Property of 4-(1,3-Dioxo-1,3,3a,4,7,7a-hexahydro-isoindol-2-yl)-3-oxo-N-phenyl-2-(triphenyl-λ⁵-phosphanylidene)-butyramide

Chemical Property:

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Technology Process of 4-(1,3-Dioxo-1,3,3a,4,7,7a-hexahydro-isoindol-2-yl)-3-oxo-N-phenyl-2-(triphenyl-λ⁵-phosphanylidene)-butyramide

There total 1 articles about 4-(1,3-Dioxo-1,3,3a,4,7,7a-hexahydro-isoindol-2-yl)-3-oxo-N-phenyl-2-(triphenyl-λ⁵-phosphanylidene)-butyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

(N-phenyliminovinylidene)triphenylphosphorane (64448-06-2,21385-80-8) + (1,3-dioxo-1,3,3a,4,7,7a-hexahydro-2H-isoindol-2-yl)acetic acid (39059-06-8) → 4-(1,3-Dioxo-1,3,3a,4,7,7a-hexahydro-isoindol-2-yl)-3-oxo-N-phenyl-2-(triphenyl-λ5-phosphanylidene)-butyramide (108159-78-0)

Guidance literature:

In ethyl acetate; 1.) 30 min; 2.) 4 h, reflux;

DOI:10.1246/cl.1986.1527

Reference yield: 84.0%

4-(1,3-Dioxo-1,3,3a,4,7,7a-hexahydro-isoindol-2-yl)-3-oxo-N-phenyl-2-(triphenyl-λ5-phosphanylidene)-butyramide (108159-78-0) → 2-[2-Oxo-3-(triphenyl-λ5-phosphanylidene)-propyl]-3a,4,7,7a-tetrahydro-isoindole-1,3-dione (108159-80-4)

Guidance literature:

With ethanol; In toluene; for 6h; Heating;

DOI:10.1246/cl.1986.1527

upstream raw materials:

(N-phenyliminovinylidene)triphenylphosphorane

(1,3-dioxo-1,3,3a,4,7,7a-hexahydro-2H-isoindol-2-yl)acetic acid

Downstream raw materials:

2-[2-Oxo-3-(triphenyl-λ⁵-phosphanylidene)-propyl]-3a,4,7,7a-tetrahydro-isoindole-1,3-dione

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