C₄₇H₆₉ClO₉Si

Base Information

Chemical Name:C₄₇H₆₉ClO₉Si
CAS No.:934560-34-6
Molecular Formula:C₄₇H₆₉ClO₉Si
Molecular Weight:841.598
Hs Code.:

C<sub>47</sub>H<sub>69</sub>ClO<sub>9</sub>Si

Synonyms:C₄₇H₆₉ClO₉Si

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Chemical Property of C₄₇H₆₉ClO₉Si

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Technology Process of C₄₇H₆₉ClO₉Si

There total 9 articles about C₄₇H₆₉ClO₉Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 886747-44-0
4-(2,2-dimethyl-4-oxo-4H-benzo[d][1,3]dioxin-5-yl)butanal

: 934560-30-2
C₃₆H₆₂O₆Si₂

: 1730-25-2
allylmagnesium bromide

: 934560-34-6
C₄₇H₆₉ClO₉Si

: C₃₁H₃₇ClO₇

Guidance literature:: 4-(2,2-dimethyl-4-oxo-4H-benzo[d][1,3]dioxin-5-yl)butanal; allylmagnesium bromide; at -78 ℃;

C₃₆H₆₂O₆Si₂; With chloro-trimethyl-silane; In(OSO₂CF₃)3; In dichloromethane; at -78 - -40 ℃; for 4h; Further stages.;
DOI:10.1039/b616558c

Reference yield:

: 863659-96-5
2-Methyl-2-[(2R,6S)-6-(2-oxo-ethyl)-tetrahydro-pyran-2-yl]-propionic acid methyl ester

: 934560-34-6
C₄₇H₆₉ClO₉Si

Guidance literature:: Multi-step reaction with 8 steps

1.1: (+)-DIPBr / tetrahydrofuran / -78 °C

2.1: 89 percent / NaH / dimethylformamide / 0.5 h / 0 °C

3.1: 83 percent / Ti[O-(i-Pr)]4 / 48 h / Heating

4.1: osmium tetraoxide; NMO / 12 h

4.2: 90 percent / NaIO₄ / 0.5 h

5.1: 78 percent / n-BuLi; KOt-Bu; B(^dIpc)2OMe / BF₃*OEt₂ / -78 °C

6.1: 79 percent / [(N,N-dimesityl-diazol-1-ium-2-yl)(Cl)2Ru=CH(2-i-PrO)Ph] / CH₂Cl₂ / 12 h / Heating

7.1: 84 percent / 2,6-lutidine; Et₃N / 0.5 h / 0 °C

8.1: (+)-DIPBr / -78 °C

8.2: TMSCl / In(OTf)3 / CH₂Cl₂ / 4 h / 25 °C

With 2,6-dimethylpyridine; osmium(VIII) oxide; n-butyllithium; N-methyl-2-indolinone; B(^dIpc)2OMe; potassium tert-butylate; sodium hydride; triethylamine; boron trifluoride diethyl etherate; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide; 1.1: Brown allylation / 5.1: Brown crotylation / 8.1: Brown allylation / 8.2: Prins cyclization;
DOI:10.1039/b616558c

Reference yield:

: C₁₅H₂₆O₄

: 934560-34-6
C₄₇H₆₉ClO₉Si

Guidance literature:: Multi-step reaction with 7 steps

1.1: 89 percent / NaH / dimethylformamide / 0.5 h / 0 °C

2.1: 83 percent / Ti[O-(i-Pr)]4 / 48 h / Heating

3.1: osmium tetraoxide; NMO / 12 h

3.2: 90 percent / NaIO₄ / 0.5 h

4.1: 78 percent / n-BuLi; KOt-Bu; B(^dIpc)2OMe / BF₃*OEt₂ / -78 °C

5.1: 79 percent / [(N,N-dimesityl-diazol-1-ium-2-yl)(Cl)2Ru=CH(2-i-PrO)Ph] / CH₂Cl₂ / 12 h / Heating

6.1: 84 percent / 2,6-lutidine; Et₃N / 0.5 h / 0 °C

7.1: (+)-DIPBr / -78 °C

7.2: TMSCl / In(OTf)3 / CH₂Cl₂ / 4 h / 25 °C

With 2,6-dimethylpyridine; osmium(VIII) oxide; n-butyllithium; N-methyl-2-indolinone; B(^dIpc)2OMe; potassium tert-butylate; sodium hydride; triethylamine; boron trifluoride diethyl etherate; In dichloromethane; N,N-dimethyl-formamide; 4.1: Brown crotylation / 7.1: Brown allylation / 7.2: Prins cyclization;
DOI:10.1039/b616558c