Technology Process of 9,10-EPOXY-9,10-DIHYDROBENZ(j)ACEAN-THRYLENE
There total 4 articles about 9,10-EPOXY-9,10-DIHYDROBENZ(j)ACEAN-THRYLENE which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
sodium hydroxide; p-toluenesulfonyl chloride;
In
1,2-dimethoxyethane;
for 2h;
Ambient temperature;
DOI:10.1021/jm00106a010
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 1.) NaBH4, O2, 2.) pyridine / 1.) ethanol, 2.) 6 h
2: 75 percent / DDQ / benzene / 2 h / Heating
3: 100 percent / NaOCH3 / tetrahydrofuran; methanol / 0.25 h / Heating
4: 46 percent / tosyl chloride, NaOH / 1,2-dimethoxy-ethane / 2 h / Ambient temperature
With
pyridine; sodium hydroxide; sodium tetrahydroborate; oxygen; sodium methylate; p-toluenesulfonyl chloride; 2,3-dicyano-5,6-dichloro-p-benzoquinone;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane; benzene;
DOI:10.1021/jm00106a010
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 100 percent / NaOCH3 / tetrahydrofuran; methanol / 0.25 h / Heating
2: 46 percent / tosyl chloride, NaOH / 1,2-dimethoxy-ethane / 2 h / Ambient temperature
With
sodium hydroxide; sodium methylate; p-toluenesulfonyl chloride;
In
tetrahydrofuran; methanol; 1,2-dimethoxyethane;
DOI:10.1021/jm00106a010
