Technology Process of 8-(D-Glucofuranosyl)-5,7,4'-trimethoxyflavanon
There total 5 articles about 8-(D-Glucofuranosyl)-5,7,4'-trimethoxyflavanon which
guide to synthetic route it.
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synthetic route:
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119677-12-2
5,7,4'-Trimethoxy-8-<(1RS,2R,3S,4R,5R)-2,3,4,5,6-pentabenzyloxy-1-hydroxyhexyl>flavanon-ethylenacetal
- Guidance literature:
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With
hydrogen;
palladium on activated charcoal;
In
acetic acid;
for 3h;
- Guidance literature:
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Multi-step reaction with 3 steps
1: 90 percent / HC(OEt)3, Amberlit IR-120 (H+ form) / 0.5 h / 90 °C
2: 72 percent / 1.6 M n-BuLi/n-hexane / tetrahydrofuran / -70 °C
3: 70 percent / H2 / 10percent Pd/C / acetic acid / 3 h
With
n-butyllithium; hexane; Amberlit IR-120 (H+ form); hydrogen; orthoformic acid triethyl ester;
palladium on activated charcoal;
In
tetrahydrofuran; acetic acid;
- Guidance literature:
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Multi-step reaction with 4 steps
1: 75 percent / HC(OEt)3, Amberlit IR-120 (H+ form) / 0.5 h / 90 °C
2: 72 percent / N-bromosuccinimide / CCl4 / 1 h / 80 °C
3: 72 percent / 1.6 M n-BuLi/n-hexane / tetrahydrofuran / -70 °C
4: 70 percent / H2 / 10percent Pd/C / acetic acid / 3 h
With
N-Bromosuccinimide; n-butyllithium; hexane; Amberlit IR-120 (H+ form); hydrogen; orthoformic acid triethyl ester;
palladium on activated charcoal;
In
tetrahydrofuran; tetrachloromethane; acetic acid;
