Technology Process of C19H25NO9
There total 4 articles about C19H25NO9 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
acetic acid; zinc;
In
methanol; dichloromethane;
at 0 - 20 ℃;
for 1h;
Inert atmosphere;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: sodium hydrogencarbonate / water / 0.5 h / 20 °C
1.2: 4.5 h / 20 °C
2.1: pyridine / 0 - 20 °C
3.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C
4.1: zinc; acetic acid / dichloromethane; methanol / 1 h / 0 - 20 °C / Inert atmosphere
With
pyridine; boron trifluoride diethyl etherate; sodium hydrogencarbonate; acetic acid; zinc;
In
methanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C
2: zinc; acetic acid / dichloromethane; methanol / 1 h / 0 - 20 °C / Inert atmosphere
With
boron trifluoride diethyl etherate; acetic acid; zinc;
In
methanol; dichloromethane;