1-(tert-butyl-diphenyl-silanyloxymethyl)-2-(dimethyl-phenyl-silanyl)-allylamine

Base Information

Chemical Name:1-(tert-butyl-diphenyl-silanyloxymethyl)-2-(dimethyl-phenyl-silanyl)-allylamine
CAS No.:867326-76-9
Molecular Formula:C₂₈H₃₇NOSi₂
Molecular Weight:459.779
Hs Code.:

1-(<i>tert</i>-butyl-diphenyl-silanyloxymethyl)-2-(dimethyl-phenyl-silanyl)-allylamine

Synonyms:1-(tert-butyl-diphenyl-silanyloxymethyl)-2-(dimethyl-phenyl-silanyl)-allylamine

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Chemical Property of 1-(tert-butyl-diphenyl-silanyloxymethyl)-2-(dimethyl-phenyl-silanyl)-allylamine

Chemical Property:

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Technology Process of 1-(tert-butyl-diphenyl-silanyloxymethyl)-2-(dimethyl-phenyl-silanyl)-allylamine

There total 5 articles about 1-(tert-butyl-diphenyl-silanyloxymethyl)-2-(dimethyl-phenyl-silanyl)-allylamine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 867326-74-7
[1-(tert-butyl-diphenyl-silanyloxymethyl)-2-(dimethyl-phenyl-silanyl)-allyl]-carbamic acid tert-butyl ester

: 867326-76-9
1-(tert-butyl-diphenyl-silanyloxymethyl)-2-(dimethyl-phenyl-silanyl)-allylamine

Guidance literature:: With trifluoroacetic acid; In dichloromethane; at 0 ℃; for 0.5h;
DOI:10.1039/b510756c

Reference yield:

: 867326-72-5
[2-(dimethyl-phenyl-silanyl)-1-hydroxymethyl-allyl]-carbamic acid tert-butyl ester

: 867326-76-9
1-(tert-butyl-diphenyl-silanyloxymethyl)-2-(dimethyl-phenyl-silanyl)-allylamine

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / imidazole / dimethylformamide / 16 h / 20 °C

2: 93 percent / TFA / CH₂Cl₂ / 0.5 h / 0 °C

With 1H-imidazole; trifluoroacetic acid; In dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b510756c

Reference yield:

: 867326-71-4
[1-(tert-butyl-dimethyl-silanyloxymethyl)-2-(dimethyl-phenyl-silanyl)-allyl]-carbamic acid tert-butyl ester

: 867326-76-9
1-(tert-butyl-diphenyl-silanyloxymethyl)-2-(dimethyl-phenyl-silanyl)-allylamine

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / TBAF / tetrahydrofuran / 0.08 h

2: 93 percent / imidazole / dimethylformamide / 16 h / 20 °C

3: 93 percent / TFA / CH₂Cl₂ / 0.5 h / 0 °C

With 1H-imidazole; tetrabutyl ammonium fluoride; trifluoroacetic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/b510756c