ethyl 3-(2-{2-(ethyloxy)-1-[2-(methyloxy)phenyl]-2-oxoethylidene}hydrazino)-3-oxopropanoate

Base Information

Chemical Name:ethyl 3-(2-{2-(ethyloxy)-1-[2-(methyloxy)phenyl]-2-oxoethylidene}hydrazino)-3-oxopropanoate
CAS No.:1040544-83-9
Molecular Formula:C₁₆H₂₀N₂O₆
Molecular Weight:336.345
Hs Code.:

Synonyms:ethyl 3-(2-{2-(ethyloxy)-1-[2-(methyloxy)phenyl]-2-oxoethylidene}hydrazino)-3-oxopropanoate

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Chemical Property of ethyl 3-(2-{2-(ethyloxy)-1-[2-(methyloxy)phenyl]-2-oxoethylidene}hydrazino)-3-oxopropanoate

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Technology Process of ethyl 3-(2-{2-(ethyloxy)-1-[2-(methyloxy)phenyl]-2-oxoethylidene}hydrazino)-3-oxopropanoate

There total 1 articles about ethyl 3-(2-{2-(ethyloxy)-1-[2-(methyloxy)phenyl]-2-oxoethylidene}hydrazino)-3-oxopropanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 30866-24-1
ethyl 3-hydrazino-3-oxopropanoate

: 16750-63-3
2-methoxyphenylmagnesium bromide

: 95-92-1
oxalic acid diethyl ester

: 1040544-83-9
ethyl 3-(2-{2-(ethyloxy)-1-[2-(methyloxy)phenyl]-2-oxoethylidene}hydrazino)-3-oxopropanoate

Guidance literature:: 2-methoxyphenylmagnesium bromide; oxalic acid diethyl ester; In tetrahydrofuran; diethyl ether; at -78 ℃; for 2h;

With hydrogenchloride; In tetrahydrofuran; diethyl ether; water; at 0 ℃;

ethyl 3-hydrazino-3-oxopropanoate; With magnesium sulfate; acetic acid; In ethanol; Heating / reflux;

Reference yield: 22.0%

: 1040544-83-9
ethyl 3-(2-{2-(ethyloxy)-1-[2-(methyloxy)phenyl]-2-oxoethylidene}hydrazino)-3-oxopropanoate

: 1040544-88-4
ethyl 5-hydroxy-6-[2-(methyloxy)phenyl]-3-oxo-2,3-dihydro-4-pyridazinecarboxylate

Guidance literature:: ethyl 3-(2-{2-(ethyloxy)-1-[2-(methyloxy)phenyl]-2-oxoethylidene}hydrazino)-3-oxopropanoate; With potassium hexamethylsilazane; In 1,4-dioxane; at 20 ℃; for 4h; Heating / reflux;

With hydrogenchloride; In 1,4-dioxane; water; at 20 ℃;