2-methoxy-5-nitro-4-phenylhydrazone of ethyl 2-oxobutenoate

Base Information

Chemical Name:2-methoxy-5-nitro-4-phenylhydrazone of ethyl 2-oxobutenoate
CAS No.:106994-16-5
Molecular Formula:C₁₇H₂₄N₄O₇S
Molecular Weight:428.466
Hs Code.:

2-methoxy-5-nitro-4-<N-(2-propenyl)methanesulfonamido>phenylhydrazone of ethyl 2-oxobutenoate

Synonyms:2-methoxy-5-nitro-4-phenylhydrazone of ethyl 2-oxobutenoate

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Chemical Property of 2-methoxy-5-nitro-4-phenylhydrazone of ethyl 2-oxobutenoate

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Technology Process of 2-methoxy-5-nitro-4-phenylhydrazone of ethyl 2-oxobutenoate

There total 14 articles about 2-methoxy-5-nitro-4-phenylhydrazone of ethyl 2-oxobutenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 58.0%

: 116911-57-0
2-[4-(Allyl-methanesulfonyl-amino)-2-methoxy-5-nitro-phenylazo]-2-ethyl-3-oxo-butyric acid ethyl ester

: 106994-16-5
2-methoxy-5-nitro-4-phenylhydrazone of ethyl 2-oxobutenoate

Guidance literature:: With sodium carbonate; In ethanol; for 8h; Ambient temperature;
DOI:10.1021/jo00256a036

Reference yield:

: 93-27-6
5-nitro-2-acetylaminoanisole

: 106994-16-5
2-{[4-(Allyl-methanesulfonyl-amino)-2-methoxy-5-nitro-phenyl]-hydrazono}-butyric acid ethyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) H₂ / 1.) Pd-C / 2.) pyridine

2: HNO₃, Hg(OAc)2 / acetic acid; acetic anhydride

3: KOC(CH₃)3 / dimethylformamide

4: H₂O, NaOH / ethanol

5: NaNO₂, HCl

6: 1.) KOH; 2.) Na₂CO₃ / 2.) EtOH

With hydrogenchloride; potassium hydroxide; sodium hydroxide; potassium tert-butylate; mercury(II) diacetate; water; hydrogen; nitric acid; sodium carbonate; sodium nitrite; palladium on activated charcoal; In ethanol; acetic anhydride; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)84617-1

Reference yield:

: 97-52-9
2-methoxy-4-nitrophenylamine

: 106994-16-5
2-{[4-(Allyl-methanesulfonyl-amino)-2-methoxy-5-nitro-phenyl]-hydrazono}-butyric acid ethyl ester

Guidance literature:: Multi-step reaction with 7 steps

1: pyridine

2: 1.) H₂ / 1.) Pd-C / 2.) pyridine

3: HNO₃, Hg(OAc)2 / acetic acid; acetic anhydride

4: KOC(CH₃)3 / dimethylformamide

5: H₂O, NaOH / ethanol

6: NaNO₂, HCl

7: 1.) KOH; 2.) Na₂CO₃ / 2.) EtOH

With hydrogenchloride; potassium hydroxide; sodium hydroxide; potassium tert-butylate; mercury(II) diacetate; water; hydrogen; nitric acid; sodium carbonate; sodium nitrite; palladium on activated charcoal; In pyridine; ethanol; acetic anhydride; acetic acid; N,N-dimethyl-formamide;
DOI:10.1016/S0040-4039(00)84617-1