phenethyl 2,3,4,2',3',4'-O-hexaacetyl-α-L-arabinopyranosyl-(1->6)-β-D-glucopyranoside

Base Information

Chemical Name:phenethyl 2,3,4,2',3',4'-O-hexaacetyl-α-L-arabinopyranosyl-(1->6)-β-D-glucopyranoside
CAS No.:860648-10-8
Molecular Formula:C₃₁H₄₀O₁₆
Molecular Weight:668.649
Hs Code.:

Synonyms:phenethyl 2,3,4,2',3',4'-O-hexaacetyl-α-L-arabinopyranosyl-(1->6)-β-D-glucopyranoside

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Chemical Property of phenethyl 2,3,4,2',3',4'-O-hexaacetyl-α-L-arabinopyranosyl-(1->6)-β-D-glucopyranoside

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Technology Process of phenethyl 2,3,4,2',3',4'-O-hexaacetyl-α-L-arabinopyranosyl-(1->6)-β-D-glucopyranoside

There total 6 articles about phenethyl 2,3,4,2',3',4'-O-hexaacetyl-α-L-arabinopyranosyl-(1->6)-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 860648-09-5
phenethyl 2,3,4-tri-O-acetyl-β-D-glucopyranoside

: 51830-02-5
bromo-2,3,4-O-triacetyl-α/β-L-arabinopyranoside

: 860648-10-8
phenethyl 2,3,4,2',3',4'-O-hexaacetyl-α-L-arabinopyranosyl-(1->6)-β-D-glucopyranoside

Guidance literature:: With silver trifluoromethanesulfonate; tetramethylurea; In dichloromethane; at 20 ℃; for 2.5h;
DOI:10.3987/COM-05-10383

Reference yield:

: 860648-07-3
phenethyl 6-O-trityl-β-D-glucopyranoside

: 860648-10-8
phenethyl 2,3,4,2',3',4'-O-hexaacetyl-α-L-arabinopyranosyl-(1->6)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 99 percent / 4-N,N-dimethylaminopyridine (DMAP) / pyridine / 1 h / 20 °C

2: 97 percent / H₂ / Pd(OH)2-C / methanol

3: 73 percent / tetramethyl urea (TMU); silver triflate (AgOTf) / CH₂Cl₂ / 2.5 h / 20 °C

With dmap; hydrogen; silver trifluoromethanesulfonate; tetramethylurea; palladium hydroxide - carbon; In pyridine; methanol; dichloromethane;
DOI:10.3987/COM-05-10383

Reference yield:

: 860648-08-4
phenethyl 2,3,4-tri-O-acetyl-6-O-trityl-β-D-glucopyranoside

: 860648-10-8
phenethyl 2,3,4,2',3',4'-O-hexaacetyl-α-L-arabinopyranosyl-(1->6)-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 97 percent / H₂ / Pd(OH)2-C / methanol

2: 73 percent / tetramethyl urea (TMU); silver triflate (AgOTf) / CH₂Cl₂ / 2.5 h / 20 °C

With hydrogen; silver trifluoromethanesulfonate; tetramethylurea; palladium hydroxide - carbon; In methanol; dichloromethane;
DOI:10.3987/COM-05-10383