C₄₅H₄₈F₄N₆O₄

Base Information

Chemical Name:C₄₅H₄₈F₄N₆O₄
CAS No.:1613055-72-3
Molecular Formula:C₄₅H₄₈F₄N₆O₄
Molecular Weight:812.908
Hs Code.:

C<sub>45</sub>H<sub>48</sub>F<sub>4</sub>N<sub>6</sub>O<sub>4</sub>

Synonyms:C₄₅H₄₈F₄N₆O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₄₅H₄₈F₄N₆O₄

Chemical Property:

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Technology Process of C₄₅H₄₈F₄N₆O₄

There total 14 articles about C₄₅H₄₈F₄N₆O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 55.0%

: 1613055-67-6
C₃₀H₃₀F₅N₃O₅S

: 1613055-70-1
C₂₂H₃₀BF₂N₃O₄

: 1613055-72-3
C₄₅H₄₈F₄N₆O₄

Guidance literature:: With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In 1,2-dimethoxyethane; water; at 90 ℃; for 3h; Inert atmosphere; Sealed tube;

Reference yield:

: 74844-91-0,114676-69-6,135042-17-0,227935-38-8,102195-79-9
(2S,4S)-N-tert-butoxycarbonyl-4-hydroxyproline methyl ester

: 1613055-72-3
C₄₅H₄₈F₄N₆O₄

Guidance literature:: Multi-step reaction with 7 steps

1.1: Dess-Martin periodane / dichloromethane / 7 h / 0 - 20 °C / Inert atmosphere; Sealed tube

2.1: diethylamino-sulfur trifluoride / dichloromethane / 21 h / -78 - 20 °C / Inert atmosphere; Sealed tube

3.1: lithium hydroxide; water / tetrahydrofuran / 2 h / 0 - 20 °C / Inert atmosphere; Sealed tube

4.1: N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate / tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere; Sealed tube

4.2: 4 h / 20 °C / Inert atmosphere; Sealed tube

5.1: acetic acid / 40 °C / Inert atmosphere; Sealed tube

6.1: dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; potassium acetate / N,N-dimethyl-formamide / 3 h / 90 °C / Inert atmosphere; Sealed tube

7.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 3 h / 90 °C / Inert atmosphere; Sealed tube

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II)*CH₂Cl₂; diethylamino-sulfur trifluoride; water; potassium acetate; potassium carbonate; Dess-Martin periodane; acetic acid; N-ethyl-N,N-diisopropylamine; N-[(dimethylamino)-3-oxo-1H-1,2,3-triazolo[4,5-b]pyridin-1-yl-methylene]-N-methylmethanaminium hexafluorophosphate; lithium hydroxide; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; N,N-dimethyl-formamide;

Reference yield:

: 1612236-53-9
C₁₂H₁₄O

: 1613055-72-3
C₄₅H₄₈F₄N₆O₄

Guidance literature:: Multi-step reaction with 5 steps

1.1: N-iodo-succinimide / tetrahydrofuran; acetonitrile / 0.17 h / Inert atmosphere; Sealed tube

1.2: 5 h / 20 °C / Inert atmosphere; Sealed tube

2.1: boron tribromide / dichloromethane / 4.16 h / -78 - 20 °C / Inert atmosphere; Sealed tube

3.1: pyridine / dichloromethane / 0.17 h / 0 °C / Inert atmosphere; Sealed tube

3.2: 1 h / 0 - 20 °C / Inert atmosphere; Sealed tube

4.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 2 h / 90 °C / Inert atmosphere; Sealed tube

5.1: potassium carbonate; tetrakis(triphenylphosphine) palladium⁽⁰⁾ / water; 1,2-dimethoxyethane / 3 h / 90 °C / Inert atmosphere; Sealed tube

With pyridine; N-iodo-succinimide; tetrakis(triphenylphosphine) palladium⁽⁰⁾; boron tribromide; potassium carbonate; In tetrahydrofuran; 1,2-dimethoxyethane; dichloromethane; water; acetonitrile;