5-(1-Hexyl-cyclopentyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-benzene-1,3-diol

Base Information

Chemical Name:5-(1-Hexyl-cyclopentyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-benzene-1,3-diol
CAS No.:1025965-31-4
Molecular Formula:C₂₇H₄₀O₂
Molecular Weight:396.613
Hs Code.:

Synonyms:5-(1-Hexyl-cyclopentyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-benzene-1,3-diol

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Chemical Property of 5-(1-Hexyl-cyclopentyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-benzene-1,3-diol

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Technology Process of 5-(1-Hexyl-cyclopentyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-benzene-1,3-diol

There total 7 articles about 5-(1-Hexyl-cyclopentyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-benzene-1,3-diol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 861892-40-2
(4R)-1-methyl-4-(2-(1-propylene))-2-cyclohexene-2-ol

: 487578-68-7
5-(1-hexylcyclopentyl)resorcinol

: 1025965-31-4
5-(1-Hexyl-cyclopentyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-benzene-1,3-diol

Guidance literature:: With toluene-4-sulfonic acid; In benzene; at 10 - 20 ℃; for 1h;
DOI:10.1021/jm020558c

Reference yield:

: 29541-98-8,55317-64-1
pentylidenetriphenylphosphorane

: 1025965-31-4
5-(1-Hexyl-cyclopentyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-benzene-1,3-diol

Guidance literature:: Multi-step reaction with 4 steps

1: 96 percent / tetrahydrofuran / 0.75 h / 10 °C

2: 95 percent / H₂ / Pd/C / ethyl acetate / 20 °C

3: 90 percent / BBr₃ / CH₂Cl₂ / 120 h / -20 °C

4: 85 percent / p-toluenesulfonic acid / benzene / 1 h / 10 - 20 °C

With hydrogen; boron tribromide; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; benzene; 1: Wittig olefination;
DOI:10.1021/jm020558c

Reference yield:

: 21406-61-1
pentyltriphenylphosphonium bromide

: 1025965-31-4
5-(1-Hexyl-cyclopentyl)-2-((1R,6R)-6-isopropenyl-3-methyl-cyclohex-2-enyl)-benzene-1,3-diol

Guidance literature:: Multi-step reaction with 5 steps

1: potassium bis(trimethylsilyl)amide / tetrahydrofuran / 30 h / 10 °C

2: 96 percent / tetrahydrofuran / 0.75 h / 10 °C

3: 95 percent / H₂ / Pd/C / ethyl acetate / 20 °C

4: 90 percent / BBr₃ / CH₂Cl₂ / 120 h / -20 °C

5: 85 percent / p-toluenesulfonic acid / benzene / 1 h / 10 - 20 °C

With hydrogen; boron tribromide; potassium hexamethylsilazane; toluene-4-sulfonic acid; palladium on activated charcoal; In tetrahydrofuran; dichloromethane; ethyl acetate; benzene; 2: Wittig olefination;
DOI:10.1021/jm020558c