tert-butyl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate

Base Information

Chemical Name:tert-butyl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate
CAS No.:1161880-99-4
Molecular Formula:C₂₂H₂₅BrN₄O₇
Molecular Weight:537.367
Hs Code.:

Synonyms:tert-butyl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate

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Chemical Property of tert-butyl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate

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Technology Process of tert-butyl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate

There total 1 articles about tert-butyl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 1161880-94-9
2-(2-bromo-3,5-dinitrophenyl)ethanamine hydrochloride

: 13734-34-4
N-tert-butoxycarbonyl-L-phenylalanine

: 1161880-99-4
tert-butyl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate

Guidance literature:: N-tert-butoxycarbonyl-L-phenylalanine; With 4-methyl-morpholine; isobutyl chloroformate; In dichloromethane; at -20 ℃; for 1h; Inert atmosphere;

2-(2-bromo-3,5-dinitrophenyl)ethanamine hydrochloride; With triethylamine; In dichloromethane; N,N-dimethyl-formamide; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo900442p

Reference yield: 81.0%

: 1161880-99-4
tert-butyl (S)-1-(2-bromo-3,5-dinitrophenethylcarbamoyl)-2-phenylethylcarbamate

: 1161881-24-8
tert-butyl (S)-1-(5,7-dinitroindolin-1-yl)-1-oxo-3-phenylpropan-2-ylcarbamate

Guidance literature:: With potassium carbonate; bis(dibenzylideneacetone)-palladium⁽⁰⁾; 2-(dicyclohexylphosphino)-2'-methylbiphenyl; In toluene; acetonitrile; at 100 ℃; Inert atmosphere; Microwave irradiation;
DOI:10.1021/jo900442p