7-(3,5-Di-tert-butylphenyl)-2-(2-tert-butylacridinyl-9-yl)-12-(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Base Information

Chemical Name:7-(3,5-Di-tert-butylphenyl)-2-(2-tert-butylacridinyl-9-yl)-12-(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine
CAS No.:118656-31-8
Molecular Formula:C₆₇H₆₃N₃O₂
Molecular Weight:942.256
Hs Code.:

7-(3,5-Di-tert-butylphenyl)-2-(2-tert-butylacridinyl-9-yl)-12-(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenz<c,h>acridine

Synonyms:7-(3,5-Di-tert-butylphenyl)-2-(2-tert-butylacridinyl-9-yl)-12-(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

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Chemical Property of 7-(3,5-Di-tert-butylphenyl)-2-(2-tert-butylacridinyl-9-yl)-12-(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

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Technology Process of 7-(3,5-Di-tert-butylphenyl)-2-(2-tert-butylacridinyl-9-yl)-12-(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

There total 3 articles about 7-(3,5-Di-tert-butylphenyl)-2-(2-tert-butylacridinyl-9-yl)-12-(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 17610-00-3
3,5-Di-tert-butylbenzaldehyde

: 118656-31-8
7-(3,5-Di-tert-butylphenyl)-2-(2-tert-butylacridinyl-9-yl)-12-(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / CH₃ONa / methanol / 2.5 h / 70 - 80 °C

2: 1.) boron trifluoride etherate, 2.) NH₃ / 1.) 110 deg C, 2.5 h, 2.) CH₂Cl₂, CH₃OH, room temp., overnight

With boron trifluoride diethyl etherate; ammonia; sodium methylate; In methanol;
DOI:10.1021/ja00186a035

Reference yield:

: C₁₅H₁₂NO₃^(1-)*Li⁽¹⁺⁾

: 118656-31-8
7-(3,5-Di-tert-butylphenyl)-2-(2-tert-butylacridinyl-9-yl)-12-(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Guidance literature:: Multi-step reaction with 2 steps

2: 1.) boron trifluoride etherate, 2.) NH₃ / 1.) 110 deg C, 2.5 h, 2.) CH₂Cl₂, CH₃OH, room temp., overnight

With boron trifluoride diethyl etherate; ammonia;
DOI:10.1021/ja00186a035

Reference yield:

: 118656-09-0
7-(2,5-Dimethoxyacridin-9-yl)-1-oxo-1,2,3,4-tetrahydronaphthalene

: 111773-18-3
2-(3,5-Di-tert-butylbenzylidene)-7-(2-tert-butylacridin-9-yl)-1-oxo-1,2,3,4-tetrahydronaphthalene

: 118656-31-8
7-(3,5-Di-tert-butylphenyl)-2-(2-tert-butylacridinyl-9-yl)-12-(2,5-dimethoxyacridin-9-yl)-5,6,8,9-tetrahydrodibenzacridine

Guidance literature:: With boron trifluoride diethyl etherate; ammonia; Yield given. Multistep reaction; 1.) 110 deg C, 2.5 h, 2.) CH₂Cl₂, CH₃OH, room temp., overnight;
DOI:10.1021/ja00186a035