1-(cyclopentylidene(4-(trifluoromethyl)phenyl)methyl)-3,5 dimethoxybenzene

Base Information

Chemical Name:1-(cyclopentylidene(4-(trifluoromethyl)phenyl)methyl)-3,5 dimethoxybenzene
CAS No.:1398416-02-8
Molecular Formula:C₂₁H₂₁F₃O₂
Molecular Weight:362.392
Hs Code.:

Synonyms:1-(cyclopentylidene(4-(trifluoromethyl)phenyl)methyl)-3,5 dimethoxybenzene

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Chemical Property of 1-(cyclopentylidene(4-(trifluoromethyl)phenyl)methyl)-3,5 dimethoxybenzene

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Technology Process of 1-(cyclopentylidene(4-(trifluoromethyl)phenyl)methyl)-3,5 dimethoxybenzene

There total 2 articles about 1-(cyclopentylidene(4-(trifluoromethyl)phenyl)methyl)-3,5 dimethoxybenzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 1398415-62-7
1-(6-iodohex-1-yn-1-yl)-4-(trifluoromethyl)benzene

: 1398416-31-3
C₁₄H₁₃BO₄

: 1398416-02-8
1-(cyclopentylidene(4-(trifluoromethyl)phenyl)methyl)-3,5 dimethoxybenzene

Guidance literature:: With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; tri(4-chlorophenyl)phosphine; In benzene; at 85 ℃; for 36h; Inert atmosphere;
DOI:10.1021/ja307761f

Reference yield:

: 705-31-7
4-trifluoromethylphenylacetylene

: 1398416-02-8
1-(cyclopentylidene(4-(trifluoromethyl)phenyl)methyl)-3,5 dimethoxybenzene

Guidance literature:: Multi-step reaction with 3 steps

1.1: n-butyllithium / tetrahydrofuran; hexane / 2.08 h / 20 °C / Inert atmosphere; Reflux

1.2: 16 h / Inert atmosphere; Reflux

2.1: sodium iodide / acetone / 4 h / Inert atmosphere; Reflux

3.1: tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; caesium carbonate; tri(4-chlorophenyl)phosphine / benzene / 36 h / 85 °C / Inert atmosphere

With tris-(dibenzylideneacetone)dipalladium⁽⁰⁾; n-butyllithium; caesium carbonate; tri(4-chlorophenyl)phosphine; sodium iodide; In tetrahydrofuran; hexane; acetone; benzene;
DOI:10.1021/ja307761f