3-methyl-1-vinylbutyl benzyloxyacetate

Base Information

• Chemical Name: 3-methyl-1-vinylbutyl benzyloxyacetate
• CAS No.: 125664-86-0
• Molecular Formula: C₁₆H₂₂O₃
• Molecular Weight: 262.349
• Mol file: 125664-86-0.mol

Synonyms:3-methyl-1-vinylbutyl benzyloxyacetate

Chemical Property of 3-methyl-1-vinylbutyl benzyloxyacetate

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3-methyl-1-vinylbutyl benzyloxyacetate

There total 2 articles about 3-methyl-1-vinylbutyl benzyloxyacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

5-methylhex-1-en-3-ol (4798-46-3) + Benzyloxyacetyl chloride (19810-31-2) → 3-methyl-1-vinylbutyl benzyloxyacetate (125664-86-0)

Guidance literature:

With pyridine; dmap; In diethyl ether;

Reference yield:

isovaleraldehyde (590-86-3) → 3-methyl-1-vinylbutyl benzyloxyacetate (125664-86-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 79 percent / tetrahydrofuran / 4 h / Ambient temperature

2: 96 percent / pyridine, DMAP / diethyl ether

With pyridine; dmap; In tetrahydrofuran; diethyl ether;

Reference yield: 65.0%

3-methyl-1-vinylbutyl benzyloxyacetate (125664-86-0) → E-2-benzyloxy-7-methyl-4-octenoic acid (125641-75-0)

Guidance literature:

With chloro-trimethyl-silane; lithium diisopropyl amide; In tetrahydrofuran; 1) -100 deg C, 10 min, 2) warm to RT, 2 h;

upstream raw materials:

5-methylhex-1-en-3-ol

Benzyloxyacetyl chloride

isovaleraldehyde

Downstream raw materials:

E-2-benzyloxy-7-methyl-4-octenoic acid

Refernces