2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1->6)]-5-O-acetyl-1,2-O-isopropylidene-α-D-glucofuranose

Base Information

Chemical Name:2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1->6)]-5-O-acetyl-1,2-O-isopropylidene-α-D-glucofuranose
CAS No.:612060-35-2
Molecular Formula:C₅₇H₆₀O₂₄
Molecular Weight:1129.09
Hs Code.:

Synonyms:2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1->6)]-5-O-acetyl-1,2-O-isopropylidene-α-D-glucofuranose

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Chemical Property of 2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1->6)]-5-O-acetyl-1,2-O-isopropylidene-α-D-glucofuranose

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Technology Process of 2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1->6)]-5-O-acetyl-1,2-O-isopropylidene-α-D-glucofuranose

There total 4 articles about 2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1->6)]-5-O-acetyl-1,2-O-isopropylidene-α-D-glucofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.8%

: 612060-34-1
3-O-allyl-2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1->6)]-5-O-acetyl-1,2-O-isopropylidene-α-D-glucofuranose

: 612060-35-2
2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1->6)]-5-O-acetyl-1,2-O-isopropylidene-α-D-glucofuranose

Guidance literature:: With methanol; palladium dichloride; at 20 ℃; for 3h;
DOI:10.1016/S0008-6215(03)00263-5

Reference yield:

: 183901-63-5
2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl trichloroacetimidate

: 612060-35-2
2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1->6)]-5-O-acetyl-1,2-O-isopropylidene-α-D-glucofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / Me₃SiOTf / CH₂Cl₂ / 3 h / -20 - 20 °C

2: 81 percent / pyridine / 24 h / 60 - 70 °C

3: 39 percent / PdCl₂ / methanol / 3 h / 20 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; palladium dichloride; In methanol; dichloromethane;
DOI:10.1081/CAR-200045260

Reference yield:

: 483361-29-1
3-O-allyl-2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-1,2-O-isopropylidene-α-D-glucofuranose

: 612060-35-2
2,4,6-tri-O-acetyl-β-D-glucopyranosyl-(1->3)-[2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl-(1->6)]-5-O-acetyl-1,2-O-isopropylidene-α-D-glucofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / Me₃SiOTf / CH₂Cl₂ / 3 h / -20 - 20 °C

2: 81 percent / pyridine / 24 h / 60 - 70 °C

3: 39 percent / PdCl₂ / methanol / 3 h / 20 °C

With pyridine; trimethylsilyl trifluoromethanesulfonate; palladium dichloride; In methanol; dichloromethane;
DOI:10.1081/CAR-200045260