1-(N₃-fluorenylmethyloxycarbonylthioureido)-N₅-(tritylaminooxyacetyl)-5-aminonaphthalene

Base Information

• Chemical Name: 1-(N₃-fluorenylmethyloxycarbonylthioureido)-N₅-(tritylaminooxyacetyl)-5-aminonaphthalene
• CAS No.: 1166232-70-7
• Molecular Formula: C₄₇H₃₈N₄O₄S
• Molecular Weight: 754.909

Synonyms:1-(N₃-fluorenylmethyloxycarbonylthioureido)-N₅-(tritylaminooxyacetyl)-5-aminonaphthalene

Chemical Property of 1-(N₃-fluorenylmethyloxycarbonylthioureido)-N₅-(tritylaminooxyacetyl)-5-aminonaphthalene

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Technology Process of 1-(N₃-fluorenylmethyloxycarbonylthioureido)-N₅-(tritylaminooxyacetyl)-5-aminonaphthalene

There total 1 articles about 1-(N₃-fluorenylmethyloxycarbonylthioureido)-N₅-(tritylaminooxyacetyl)-5-aminonaphthalene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

N1-(tritylaminooxyacetyl)-1,5-diaminonaphthalene (1166232-40-1) + 9-fluorenylmethoxycarbonyl isothiocyanate (199915-38-3) → 1-(N3-fluorenylmethyloxycarbonylthioureido)-N5-(tritylaminooxyacetyl)-5-aminonaphthalene (1166232-70-7)

Guidance literature:

In dichloromethane; at 0 - 20 ℃;

DOI:10.1021/ja904767k

Reference yield: 85.0%

1-(N3-fluorenylmethyloxycarbonylthioureido)-N5-(tritylaminooxyacetyl)-5-aminonaphthalene (1166232-70-7) + N-(8-amino-3,6-dioxaoctanyl)biotinamide (138529-46-1) → 1-(N3-{2-[2-(2-biotinylaminoethoxy)ethoxy]ethyl}-N2-fluorenylmethyloxycarbonylguanidino)-N5-(tritylaminooxyacetyl)-5-aminonaphthalene (1166232-73-0)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; mercury dichloride; In N,N-dimethyl-formamide; at 0 ℃;

DOI:10.1021/ja904767k

upstream raw materials:

N₁-(tritylaminooxyacetyl)-1,5-diaminonaphthalene

9-fluorenylmethoxycarbonyl isothiocyanate

Downstream raw materials:

1-(N₃-{2-[2-(2-biotinylaminoethoxy)ethoxy]ethyl}-N₂-fluorenylmethyloxycarbonylguanidino)-N₅-(tritylaminooxyacetyl)-5-aminonaphthalene

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